N-[(4-nitrophenyl)methyl]-N-{[4-(trifluoromethyl)phenyl]methyl}-1-propanamine

Base Information

Chemical Name:N-[(4-nitrophenyl)methyl]-N-{[4-(trifluoromethyl)phenyl]methyl}-1-propanamine
CAS No.:1508310-57-3
Molecular Formula:C₁₈H₁₉F₃N₂O₂
Molecular Weight:352.356
Hs Code.:

Synonyms:N-[(4-nitrophenyl)methyl]-N-{[4-(trifluoromethyl)phenyl]methyl}-1-propanamine

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Chemical Property of N-[(4-nitrophenyl)methyl]-N-{[4-(trifluoromethyl)phenyl]methyl}-1-propanamine

Chemical Property:

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Technology Process of N-[(4-nitrophenyl)methyl]-N-{[4-(trifluoromethyl)phenyl]methyl}-1-propanamine

There total 3 articles about N-[(4-nitrophenyl)methyl]-N-{[4-(trifluoromethyl)phenyl]methyl}-1-propanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 90390-13-9
N-{[4-(trifluoromethyl)phenyl]methyl}-1-propanamine

: 1508310-57-3
N-[(4-nitrophenyl)methyl]-N-{[4-(trifluoromethyl)phenyl]methyl}-1-propanamine

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃;
DOI:10.1021/ml4003875

Reference yield:

: Propyl-[1-(4-trifluoromethyl-phenyl)-meth-(E)-ylidene]-amine

: 1508310-57-3
N-[(4-nitrophenyl)methyl]-N-{[4-(trifluoromethyl)phenyl]methyl}-1-propanamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 1.5 h / Inert atmosphere

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

With sodium tetrahydroborate; sodium tris(acetoxy)borohydride; In methanol; 1,2-dichloro-ethane;
DOI:10.1021/ml4003875

Reference yield:

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 1508310-57-3
N-[(4-nitrophenyl)methyl]-N-{[4-(trifluoromethyl)phenyl]methyl}-1-propanamine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium sulfate / dichloromethane / 72 h / 20 °C

2: sodium tetrahydroborate / methanol / 1.5 h / Inert atmosphere

3: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

With sodium tetrahydroborate; sodium tris(acetoxy)borohydride; sodium sulfate; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ml4003875