di-tert-butyl [[4-(5-amidinobenzofuran-2-carboxamido)-o-phenylene]dioxy]diacetate

Base Information

Chemical Name:di-tert-butyl [[4-(5-amidinobenzofuran-2-carboxamido)-o-phenylene]dioxy]diacetate
CAS No.:259150-10-2
Molecular Formula:C₂₈H₃₃N₃O₈
Molecular Weight:539.585
Hs Code.:

Synonyms:di-tert-butyl [[4-(5-amidinobenzofuran-2-carboxamido)-o-phenylene]dioxy]diacetate

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Chemical Property of di-tert-butyl [[4-(5-amidinobenzofuran-2-carboxamido)-o-phenylene]dioxy]diacetate

Chemical Property:

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Technology Process of di-tert-butyl [[4-(5-amidinobenzofuran-2-carboxamido)-o-phenylene]dioxy]diacetate

There total 5 articles about di-tert-butyl [[4-(5-amidinobenzofuran-2-carboxamido)-o-phenylene]dioxy]diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026085-15-3
{2-tert-butoxycarbonylmethoxy-5-[(5-methylsulfanylcarbonimidoyl-benzofuran-2-carbonyl)-amino]-phenoxy}-acetic acid tert-butyl ester

: 259150-10-2
di-tert-butyl [[4-(5-amidinobenzofuran-2-carboxamido)-o-phenylene]dioxy]diacetate

Guidance literature:: With ammonium acetate; In methanol; for 3h; Heating;
DOI:10.1248/cpb.47.1694

Reference yield:

: 84102-75-0
5-cyanobenzo[b]furan-2-carboxylic acid

: 259150-10-2
di-tert-butyl [[4-(5-amidinobenzofuran-2-carboxamido)-o-phenylene]dioxy]diacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / HOBt; EDI / dimethylformamide / 18 h / 20 °C

2: 42 percent / H₂S; TEA / pyridine / 18 h / 20 °C

3: acetone / 0.67 h / Heating

4: ammonium acetate / methanol / 3 h / Heating

With ammonium acetate; TEA; hydrogen sulfide; benzotriazol-1-ol; In pyridine; methanol; N,N-dimethyl-formamide; acetone; 1: coupling / 2: Addition / 3: Methylation / 4: Substitution;
DOI:10.1248/cpb.47.1694

Reference yield:

: 167843-71-2
3,4-di-t-butoxycarbonylmethoxyaniline

: 259150-10-2
di-tert-butyl [[4-(5-amidinobenzofuran-2-carboxamido)-o-phenylene]dioxy]diacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / HOBt; EDI / dimethylformamide / 18 h / 20 °C

2: 42 percent / H₂S; TEA / pyridine / 18 h / 20 °C

3: acetone / 0.67 h / Heating

4: ammonium acetate / methanol / 3 h / Heating

With ammonium acetate; TEA; hydrogen sulfide; benzotriazol-1-ol; In pyridine; methanol; N,N-dimethyl-formamide; acetone; 1: coupling / 2: Addition / 3: Methylation / 4: Substitution;
DOI:10.1248/cpb.47.1694