2-(3,4-dimethoxyphenyl)-2,3,7,8-tetrahydroacenaphtho[5,6-bc]azepin-4(1H)-one

Base Information

• Chemical Name: 2-(3,4-dimethoxyphenyl)-2,3,7,8-tetrahydroacenaphtho[5,6-bc]azepin-4(1H)-one
• CAS No.: 1030384-88-3
• Molecular Formula: C₂₃H₂₁NO₃
• Molecular Weight: 359.425

Synonyms:2-(3,4-dimethoxyphenyl)-2,3,7,8-tetrahydroacenaphtho[5,6-bc]azepin-4(1H)-one

Chemical Property of 2-(3,4-dimethoxyphenyl)-2,3,7,8-tetrahydroacenaphtho[5,6-bc]azepin-4(1H)-one

Chemical Property:

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Technology Process of 2-(3,4-dimethoxyphenyl)-2,3,7,8-tetrahydroacenaphtho[5,6-bc]azepin-4(1H)-one

There total 1 articles about 2-(3,4-dimethoxyphenyl)-2,3,7,8-tetrahydroacenaphtho[5,6-bc]azepin-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-(6-aminoacenaphthen-5-yl)ethanone (5209-01-8) + 3,4-dimethoxy-benzaldehyde (120-14-9) → 2-(3,4-dimethoxyphenyl)-2,3,7,8-tetrahydroacenaphtho[5,6-bc]azepin-4(1H)-one (1030384-88-3)

Guidance literature:

With sodium hydroxide; In ethanol; water; at 50 - 60 ℃;

DOI:10.1134/S107042800707010X

Reference yield: 92.0%

2-(3,4-dimethoxyphenyl)-2,3,7,8-tetrahydroacenaphtho[5,6-bc]azepin-4(1H)-one (1030384-88-3) + methyl iodide (74-88-4) → 2-(3,4-dimethoxyphenyl)-1-methyl-1,2,3,4,7,8-hexahydroacenaphtho[5,6-bc]azepin-4-one (1101168-22-2)

Guidance literature:

With potassium carbonate; In acetonitrile; for 15h; Reflux;

DOI:10.1134/S1070428008070208

Reference yield: 87.0%

2-(3,4-dimethoxyphenyl)-2,3,7,8-tetrahydroacenaphtho[5,6-bc]azepin-4(1H)-one (1030384-88-3) → 2-(3,4-dimethoxyphenyl)-1,2,3,4,7,8-hexahydroacenaphtho[5,6-bc]azepin-4-one hydrazone (1200113-56-9)

Guidance literature:

With hydrazine hydrate; acetic acid; In ethanol; Reflux;

DOI:10.1134/S1070428009060219

upstream raw materials:

1-(6-aminoacenaphthen-5-yl)ethanone

3,4-dimethoxy-benzaldehyde

Downstream raw materials:

2-(3,4-dimethoxyphenyl)-1,2,3,4-tetrahydroacenaphtho[5,6-bc]azepin-4-one

2-(3,4-dimethoxyphenyl)-1-methyl-1,2,3,4,7,8-hexahydroacenaphtho[5,6-bc]azepin-4-one

2-(3,4-dimethoxyphenyl)-1,2,3,4,7,8-hexahydroacenaphtho[5,6-bc]azepin-4-one hydrazone

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