2-DIMETHYLAMINO-3-NITROFLUORENE

Base Information

• Chemical Name: 2-DIMETHYLAMINO-3-NITROFLUORENE
• CAS No.: 57105-64-3
• Molecular Formula: C15H14N2O2
• Molecular Weight: 254.28
• Mol file: 57105-64-3.mol

Synonyms:9H-Fluoren-2-amine,N,N-dimethyl-3-nitro;2-DIMETHYLAMINO-3-NITROFLUORENE;3-Nitro-2-dimethylamino-fluoren;

Chemical Property of 2-DIMETHYLAMINO-3-NITROFLUORENE

Chemical Property:

• Vapor Pressure: 6.27E-08mmHg at 25°C
• Boiling Point: 439.6°Cat760mmHg
• Flash Point: 219.7°C
• PSA: 49.06000
• Density: 1.283g/cm³
• LogP: 3.75520

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-DIMETHYLAMINO-3-NITROFLUORENE

There total 4 articles about 2-DIMETHYLAMINO-3-NITROFLUORENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl-2-aminofluorene (13261-62-6) → dimethyl-(1-nitro-fluoren-2-yl)-amine (108013-57-6) + 3-Nitro-2-dimethylamino-fluoren (57105-64-3)

Guidance literature:

With acetic acid; sodium nitrite;

DOI:10.1039/jr9490002020 DOI:10.1021/jo01075a017

Reference yield:

2-aminofluorene (153-78-6) → 3-Nitro-2-dimethylamino-fluoren (57105-64-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide

2: acetic acid; sodium nitrite

With sodium hydroxide; acetic acid; sodium nitrite;

DOI:10.1039/jr9490002020

Reference yield:

N,N-dimethyl-2-aminofluorene (13261-62-6) + acetic acid (64-19-7,77671-22-8) → dimethyl-(1-nitro-fluoren-2-yl)-amine (108013-57-6) + 3-Nitro-2-dimethylamino-fluoren (57105-64-3)

Guidance literature:

DOI:10.1039/jr9490002020 DOI:10.1021/jo01075a017

upstream raw materials:

N,N-dimethyl-2-aminofluorene

acetic acid

2-aminofluorene