(3S,8R,9S,10S,13S,14S,17S)-10,13-dimethyl-17-[5-methyl-4-oxo-7-(2,6,6-trimethylcyclohex-1-en-1-yl)heptanoyl]hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

Base Information

Chemical Name:(3S,8R,9S,10S,13S,14S,17S)-10,13-dimethyl-17-[5-methyl-4-oxo-7-(2,6,6-trimethylcyclohex-1-en-1-yl)heptanoyl]hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate
CAS No.:1337568-94-1
Molecular Formula:C₃₈H₆₀O₄
Molecular Weight:580.892
Hs Code.:

(3S,8R,9S,10S,13S,14S,17S)-10,13-dimethyl-17-[5-methyl-4-oxo-7-(2,6,6-trimethylcyclohex-1-en-1-yl)heptanoyl]hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

Synonyms:(3S,8R,9S,10S,13S,14S,17S)-10,13-dimethyl-17-[5-methyl-4-oxo-7-(2,6,6-trimethylcyclohex-1-en-1-yl)heptanoyl]hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

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Chemical Property of (3S,8R,9S,10S,13S,14S,17S)-10,13-dimethyl-17-[5-methyl-4-oxo-7-(2,6,6-trimethylcyclohex-1-en-1-yl)heptanoyl]hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

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Technology Process of (3S,8R,9S,10S,13S,14S,17S)-10,13-dimethyl-17-[5-methyl-4-oxo-7-(2,6,6-trimethylcyclohex-1-en-1-yl)heptanoyl]hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

There total 4 articles about (3S,8R,9S,10S,13S,14S,17S)-10,13-dimethyl-17-[5-methyl-4-oxo-7-(2,6,6-trimethylcyclohex-1-en-1-yl)heptanoyl]hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1337568-67-8
2-[2-ethoxy-3-methyl-5-(2,6,6-trimethylcyclohex-1-en-1-yl)pent-1-en-3-yl]-6-fluoropyridine

: 1337568-73-6
(3S,8R,9S,10S,13S,14S,17S)-17-{2-[(ethoxycarbonothioyl)thio]acetyl}-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

: 1337568-94-1
(3S,8R,9S,10S,13S,14S,17S)-10,13-dimethyl-17-[5-methyl-4-oxo-7-(2,6,6-trimethylcyclohex-1-en-1-yl)heptanoyl]hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

Guidance literature:: 2-[2-ethoxy-3-methyl-5-(2,6,6-trimethylcyclohex-1-en-1-yl)pent-1-en-3-yl]-6-fluoropyridine; (3S,8R,9S,10S,13S,14S,17S)-17-{2-[(ethoxycarbonothioyl)thio]acetyl}-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate; With dilauryl peroxide; In ethyl acetate; Inert atmosphere; Reflux;

With hydrogenchloride; water; In ethyl acetate; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol202399c

Reference yield:

: 1337568-65-6
C₁₇H₃₀O₂

: 1337568-94-1
(3S,8R,9S,10S,13S,14S,17S)-10,13-dimethyl-17-[5-methyl-4-oxo-7-(2,6,6-trimethylcyclohex-1-en-1-yl)heptanoyl]hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.33 h / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux

2.2: 1 h / 20 °C / Inert atmosphere

With dilauryl peroxide; sodium hydride; In dimethyl sulfoxide; ethyl acetate; mineral oil;
DOI:10.1021/ol202399c

Reference yield:

: 95671-03-7
C₂₃H₃₅BrO₃

: 1337568-94-1
(3S,8R,9S,10S,13S,14S,17S)-10,13-dimethyl-17-[5-methyl-4-oxo-7-(2,6,6-trimethylcyclohex-1-en-1-yl)heptanoyl]hexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetone / 1 h / Inert atmosphere

2.1: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux

2.2: 1 h / 20 °C / Inert atmosphere

With dilauryl peroxide; In ethyl acetate; acetone;
DOI:10.1021/ol202399c