Technology Process of C27H25NO4
There total 4 articles about C27H25NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; mineral oil;
at -15 - 20 ℃;
for 18.5h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: pyridine / isopropyl alcohol / 8 h / 80 - 82 °C
2.1: sodium hydride / tetra-(n-butyl)ammonium iodide / tetrahydrofuran; mineral oil / -15 - 20 °C / Inert atmosphere
2.2: -5 - 0 °C
With
pyridine; sodium hydride;
tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; isopropyl alcohol; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / tetra-(n-butyl)ammonium iodide / tetrahydrofuran; mineral oil / -15 - 20 °C / Inert atmosphere
2: pyridine / isopropyl alcohol / 8 h / 80 - 82 °C
3: sodium hydride / tetra-(n-butyl)ammonium iodide / tetrahydrofuran; mineral oil / 18.5 h / -15 - 20 °C
With
sodium hydride;
pyridine; tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; isopropyl alcohol; mineral oil;