(2S,3R,5S,6R)-6-((R)-hex-5-en-2-yloxy)-5-hydroxy-2-methyltetrahydro-2H-pyran-3-yl benzoate

Base Information

Chemical Name:(2S,3R,5S,6R)-6-((R)-hex-5-en-2-yloxy)-5-hydroxy-2-methyltetrahydro-2H-pyran-3-yl benzoate
CAS No.:1417721-60-8
Molecular Formula:C₁₉H₂₆O₅
Molecular Weight:334.412
Hs Code.:

Synonyms:(2S,3R,5S,6R)-6-((R)-hex-5-en-2-yloxy)-5-hydroxy-2-methyltetrahydro-2H-pyran-3-yl benzoate

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Chemical Property of (2S,3R,5S,6R)-6-((R)-hex-5-en-2-yloxy)-5-hydroxy-2-methyltetrahydro-2H-pyran-3-yl benzoate

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Technology Process of (2S,3R,5S,6R)-6-((R)-hex-5-en-2-yloxy)-5-hydroxy-2-methyltetrahydro-2H-pyran-3-yl benzoate

There total 3 articles about (2S,3R,5S,6R)-6-((R)-hex-5-en-2-yloxy)-5-hydroxy-2-methyltetrahydro-2H-pyran-3-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1417721-58-4
C₁₉H₂₄O₅

: 1417721-60-8
(2S,3R,5S,6R)-6-((R)-hex-5-en-2-yloxy)-5-hydroxy-2-methyltetrahydro-2H-pyran-3-yl benzoate

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; for 0.166667h;
DOI:10.1002/anie.201206797

Reference yield:

: 1172590-11-2
(2R,3R,5R,6S)-2-((R)-hex-5-en-2-yloxy)-6-methyltetrahydro-2H-pyran-3,5-diyl dibenzoate

: 1417721-60-8
(2S,3R,5S,6R)-6-((R)-hex-5-en-2-yloxy)-5-hydroxy-2-methyltetrahydro-2H-pyran-3-yl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide / tetrahydrofuran; water; 1,4-dioxane / 0.67 h / 60 °C

2: Dess-Martin periodane / dichloromethane / 5 h

3: sodium tetrahydroborate / methanol; dichloromethane / 0.17 h

With sodium tetrahydroborate; Dess-Martin periodane; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;
DOI:10.1002/anie.201206797

Reference yield:

: 1417721-56-2
C₁₉H₂₆O₅

: 1417721-60-8
(2S,3R,5S,6R)-6-((R)-hex-5-en-2-yloxy)-5-hydroxy-2-methyltetrahydro-2H-pyran-3-yl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 5 h

2: sodium tetrahydroborate / methanol; dichloromethane / 0.17 h

With sodium tetrahydroborate; Dess-Martin periodane; In methanol; dichloromethane;
DOI:10.1002/anie.201206797