(E)-S-3-((3-ethynyl-5-((2-(4-mercaptobutanoyl)hydrazono)methyl)phenoxy)methyl)benzylethanethioate

Base Information

Chemical Name:(E)-S-3-((3-ethynyl-5-((2-(4-mercaptobutanoyl)hydrazono)methyl)phenoxy)methyl)benzylethanethioate
CAS No.:1256478-11-1
Molecular Formula:C₂₃H₂₄N₂O₃S₂
Molecular Weight:440.587
Hs Code.:

Synonyms:(E)-S-3-((3-ethynyl-5-((2-(4-mercaptobutanoyl)hydrazono)methyl)phenoxy)methyl)benzylethanethioate

Suppliers and Price of (E)-S-3-((3-ethynyl-5-((2-(4-mercaptobutanoyl)hydrazono)methyl)phenoxy)methyl)benzylethanethioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-S-3-((3-ethynyl-5-((2-(4-mercaptobutanoyl)hydrazono)methyl)phenoxy)methyl)benzylethanethioate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (E)-S-3-((3-ethynyl-5-((2-(4-mercaptobutanoyl)hydrazono)methyl)phenoxy)methyl)benzylethanethioate

There total 4 articles about (E)-S-3-((3-ethynyl-5-((2-(4-mercaptobutanoyl)hydrazono)methyl)phenoxy)methyl)benzylethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 936923-81-8
4-mercaptobutyric acid hydrazide

: 1219077-43-6
C₁₉H₁₆O₃S

: 1256478-11-1
(E)-S-3-((3-ethynyl-5-((2-(4-mercaptobutanoyl)hydrazono)methyl)phenoxy)methyl)benzylethanethioate

Guidance literature:: With acetic acid; In methanol; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja106486b

Reference yield:

: 871345-34-5
3-ethynyl-5-hydroxybenzaldehyde

: 1256478-11-1
(E)-S-3-((3-ethynyl-5-((2-(4-mercaptobutanoyl)hydrazono)methyl)phenoxy)methyl)benzylethanethioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

2.1: triethylamine / dichloromethane / 16 h / 20 °C

2.2: 3 h / 20 °C

3.1: acetic acid / methanol / 2 h / 20 °C / Inert atmosphere

With sodium hydride; acetic acid; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja106486b

Reference yield:

: 1219077-42-5
C₁₇H₁₄O₃

: 1256478-11-1
(E)-S-3-((3-ethynyl-5-((2-(4-mercaptobutanoyl)hydrazono)methyl)phenoxy)methyl)benzylethanethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 16 h / 20 °C

1.2: 3 h / 20 °C

2.1: acetic acid / methanol / 2 h / 20 °C / Inert atmosphere

With acetic acid; triethylamine; In methanol; dichloromethane;
DOI:10.1021/ja106486b