1,3-Di-p-tolylcyclopentaceanthrylene-2(H)-one

Base Information

• Chemical Name: 1,3-Di-p-tolylcyclopent
• Molecular Formula: C₃₃H₂₂O
• Molecular Weight: 434.537

Synonyms:1,3-Di-p-tolylcyclopentaceanthrylene-2(H)-one

Chemical Property of 1,3-Di-p-tolylcyclopent

Chemical Property:

Purity/Quality:

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Useful:

There total 1 articles about 1,3-Di-p-tolylcyclopentaceanthrylene-2(H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1,3-bis(4-methylphenyl)-2-propanone (70769-70-9) + aceanthrenequinone (6373-11-1) → 1,3-Di-p-tolylcyclopentaceanthrylene-2(H)-one (83808-71-3)

Guidance literature:

With methanol-sodium hydroxide (10percent); In methanol; for 0.5h; Heating;

Reference yield: 55.0%

1,3-Di-p-tolylcyclopentaceanthrylene-2(H)-one (83808-71-3) + diphenyl acetylene (501-65-5) → 2,3-Diphenyl-1,4-di-p-tolylbenzaceanthrylene (83808-75-7)

Guidance literature:

In various solvent(s); 1.) 6 h, reflux, 2.) standing over night;

Reference yield:

maleic anhydride (108-31-6) + 1,3-Di-p-tolylcyclopentaceanthrylene-2(H)-one (83808-71-3) + bicyclo[2.2.1]hepta-2,5-diene (121-46-0) → 5-norbornene-2,3-dicarboxylic anhydride (826-62-0,85081-15-8,85081-16-9) + 1,4-Di-p-tolylbenzaceanthrylene (83808-74-6)

Guidance literature:

Yield given. Multistep reaction; 1.) xylene, boiling, 2.) ether, 4 h;

upstream raw materials:

1,3-bis(4-methylphenyl)-2-propanone

aceanthrenequinone

Downstream raw materials:

5-norbornene-2,3-dicarboxylic anhydride

1,4-Di-p-tolylbenzaceanthrylene

9,13-Di-p-tolylaceanthryleno<1,2-f>-isobenzofuran-10,12-dione

9,15-Di-p-tolyl-14H-fluoreno<2,3-a>aceanthrylene

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