2-(4-methoxyphenyl)-1-[(4-methylphenyl)sulfonyl]-4-phenyl-1H-imidazole

Base Information

• Chemical Name: 2-(4-methoxyphenyl)-1-[(4-methylphenyl)sulfonyl]-4-phenyl-1H-imidazole
• CAS No.: 1078739-28-2
• Molecular Formula: C₂₃H₂₀N₂O₃S
• Molecular Weight: 404.489

Synonyms:2-(4-methoxyphenyl)-1-[(4-methylphenyl)sulfonyl]-4-phenyl-1H-imidazole

Chemical Property of 2-(4-methoxyphenyl)-1-[(4-methylphenyl)sulfonyl]-4-phenyl-1H-imidazole

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Technology Process of 2-(4-methoxyphenyl)-1-[(4-methylphenyl)sulfonyl]-4-phenyl-1H-imidazole

There total 4 articles about 2-(4-methoxyphenyl)-1-[(4-methylphenyl)sulfonyl]-4-phenyl-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-bromo-4-phenyl-1-tosyl-1H-imidazole + 4-methoxyphenylboronic acid (5720-07-0) → 2-(4-methoxyphenyl)-1-[(4-methylphenyl)sulfonyl]-4-phenyl-1H-imidazole (1078739-28-2)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; benzene; at 80 ℃; for 20h; Inert atmosphere;

DOI:10.1021/acs.orglett.5b00977

Reference yield: 87.0%

1-(4-methylbenzensulfonyl)-4-phenyl-1H-1,2,3-triazole (884866-01-7) + 4-methoxybenzonitrile (874-90-8) → 2-(4-methoxyphenyl)-1-[(4-methylphenyl)sulfonyl]-4-phenyl-1H-imidazole (1078739-28-2)

Guidance literature:

With Rh₂[(N-(4-dodecylphenyl)sulfonyl)-(S)-prolinate]4; In 1,2-dichloro-ethane; at 80 ℃; Inert atmosphere;

DOI:10.1021/ja805079v

Reference yield: 46.0%

N-[[rel-(2R,3S)-1-(1,3-dioxoisoindol-2-yl)-3-(4-methoxylphenyl)aziridin-2-yl](phenyl)methylene]-4-methylbenzenesulfonamide → 2-(4-methoxyphenyl)-1-[(4-methylphenyl)sulfonyl]-4-phenyl-1H-imidazole (1078739-28-2)

Guidance literature:

In toluene; at 140 ℃; for 4h; regioselective reaction; Sealed tube;

DOI:10.1002/ejoc.201701806

upstream raw materials:

1-(4-methylbenzensulfonyl)-4-phenyl-1H-1,2,3-triazole

4-methoxybenzonitrile

4-methoxyphenylboronic acid

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