1-[Ir(H)(Br)(CO)(PPh3)2]-7-C6H5-1,7-(σdicarba-closo-dodecaborane(12))

Base Information

Chemical Name:1-[Ir(H)(Br)(CO)(PPh3)2]-7-C6H5-1,7-(σdicarba-closo-dodecaborane(12))
CAS No.:74333-16-7
Molecular Formula:C₄₅H₄₆B₁₀BrIrOP₂
Molecular Weight:1045.04
Hs Code.:

Synonyms:1-[Ir(H)(Br)(CO)(PPh3)2]-7-C6H5-1,7-(σdicarba-closo-dodecaborane(12))

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Chemical Property of 1-[Ir(H)(Br)(CO)(PPh3)2]-7-C6H5-1,7-(σdicarba-closo-dodecaborane(12))

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Technology Process of 1-[Ir(H)(Br)(CO)(PPh3)2]-7-C6H5-1,7-(σdicarba-closo-dodecaborane(12))

There total 1 articles about 1-[Ir(H)(Br)(CO)(PPh3)2]-7-C6H5-1,7-(σdicarba-closo-dodecaborane(12)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1-[trans-Ir(CO)(PPh3)2]-7-C6H5-1,7-(σdicarba-closo-dodecaborane(12))

: 74333-16-7
1-[Ir(H)(Br)(CO)(PPh3)2]-7-C6H5-1,7-(σdicarba-closo-dodecaborane(12))

Guidance literature:: With hydrogen bromide; In not given; Ar-atmosphere; dropwise addn. of HBr (in dry C6H6 or CH2Cl2 to soln. of Ir-complex (in dry C6H6 or CH2Cl2), stirring (1 h); pptn. on hexane addn., recrystn. (C6H6/hexane);
DOI:10.1016/S0020-1693(00)93629-6