3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:121042-74-8
Molecular Formula:C₂₂H₂₉F₃N₂O₈
Molecular Weight:506.476
Hs Code.:

Synonyms:3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Suppliers and Price of 3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 5 articles about 3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: C₂₂H₂₇F₃N₂O₈

: 121042-74-8
3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: C₂₂H₂₇F₃N₂O₈; With sodium cyanoborohydride; In tetrahydrofuran; for 0.5h; Molecular sieve;

With methanesulfonic acid; In tetrahydrofuran; for 3h; pH=3; Molecular sieve;
DOI:10.1016/j.carres.2016.09.016

Reference yield:

: 121042-72-6
Acetic acid (4aR,6R,7R,8R,8aS)-7-acetylamino-2-phenyl-6-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

: 121042-74-8
3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 8h; Yield given; molecular sieve 3 Angstroem;
DOI:10.1007/BF00598177

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 121042-74-8
3-(trifluoroacetamido)propyl 2-acetamido-3-O-acetyl-6-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1) CH₃ONa, 2) toluene-4-sulfonic acid / 1) CH₃OH, 2 h, 2) CH₃CN, 50 deg C

2: pyridine / 20 h

3: NaBH₃CN, HCl / tetrahydrofuran; diethyl ether / 8 h / 20 °C / molecular sieve 3 Angstroem

With pyridine; hydrogenchloride; sodium methylate; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether;
DOI:10.1007/BF00598177