N-{3-[(2R,3R,4R,5S)-3-Acetylamino-6-benzyloxymethyl-5-hydroxy-4-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

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Chemical Name:N-{3-[(2R,3R,4R,5S)-3-Acetylamino-6-benzyloxymethyl-5-hydroxy-4-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide
CAS No.:121042-76-0
Molecular Formula:C₂₆H₃₇F₃N₂O₁₂
Molecular Weight:626.581
Hs Code.:

N-{3-[(2R,3R,4R,5S)-3-Acetylamino-6-benzyloxymethyl-5-hydroxy-4-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

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Chemical Property of N-{3-[(2R,3R,4R,5S)-3-Acetylamino-6-benzyloxymethyl-5-hydroxy-4-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

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Technology Process of N-{3-[(2R,3R,4R,5S)-3-Acetylamino-6-benzyloxymethyl-5-hydroxy-4-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

There total 6 articles about N-{3-[(2R,3R,4R,5S)-3-Acetylamino-6-benzyloxymethyl-5-hydroxy-4-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121042-75-9
3-(trifluoroacetamido)propyl 2-acetamido-6-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-2-deoxy-β-D-glucopyranoside

: 121042-76-0
N-{3-[(2R,3R,4R,5S)-3-Acetylamino-6-benzyloxymethyl-5-hydroxy-4-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

Guidance literature:: With sodium methylate; In methanol; for 15h;
DOI:10.1007/BF00598177

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 121042-76-0
N-{3-[(2R,3R,4R,5S)-3-Acetylamino-6-benzyloxymethyl-5-hydroxy-4-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 6 steps

1: 1) CH₃ONa, 2) toluene-4-sulfonic acid / 1) CH₃OH, 2 h, 2) CH₃CN, 50 deg C

2: pyridine / 20 h

3: NaBH₃CN, HCl / tetrahydrofuran; diethyl ether / 8 h / 20 °C / molecular sieve 3 Angstroem

4: CH₃ONa / methanol / 24 h

5: mercury cyanide / nitromethane; benzene / 2 h / 50 - 60 °C / molecular sieve 4 Angstroem

6: CH₃ONa / methanol / 15 h

With pyridine; hydrogenchloride; sodium methylate; mercury(II) cyanide; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; nitromethane; benzene;
DOI:10.1007/BF00598177

Reference yield:

: 121042-73-7
3-trifluoroacetamidopropyl 2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 121042-76-0
N-{3-[(2R,3R,4R,5S)-3-Acetylamino-6-benzyloxymethyl-5-hydroxy-4-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: mercury cyanide / nitromethane; benzene / 2 h / 50 - 60 °C / molecular sieve 4 Angstroem

2: CH₃ONa / methanol / 15 h

With sodium methylate; mercury(II) cyanide; In methanol; nitromethane; benzene;
DOI:10.1007/BF00598177