4,6-Dimethyl-1-oxy-pyridine-3-sulfonic acid p-tolylamide

Base Information

• Chemical Name: 4,6-Dimethyl-1-oxy-pyridine-3-sulfonic acid p-tolylamide
• CAS No.: 184433-66-7
• Molecular Formula: C₁₄H₁₆N₂O₃S
• Molecular Weight: 292.359
• Mol file: 184433-66-7.mol

Synonyms:4,6-Dimethyl-1-oxy-pyridine-3-sulfonic acid p-tolylamide

Chemical Property of 4,6-Dimethyl-1-oxy-pyridine-3-sulfonic acid p-tolylamide

Chemical Property:

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Technology Process of 4,6-Dimethyl-1-oxy-pyridine-3-sulfonic acid p-tolylamide

There total 1 articles about 4,6-Dimethyl-1-oxy-pyridine-3-sulfonic acid p-tolylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

3,5-Dimethyl-1,1-dioxo-2-p-tolyl-1,2-dihydro-1λ6-[1,2]thiazine-6-carbaldehyde (94494-29-8) → 4,6-Dimethyl-1-oxy-pyridine-3-sulfonic acid p-tolylamide (184433-66-7)

Guidance literature:

With hydroxylamine hydrochloride; sodium carbonate; In ethanol; water; for 1h; Heating;

DOI:10.1055/s-1996-4382

Reference yield: 69.0%

4,6-Dimethyl-1-oxy-pyridine-3-sulfonic acid p-tolylamide (184433-66-7) → 2,4-Dimethyl-pyridin-5-(N-4-tolyl)-sulfonamid

Guidance literature:

With phosphorus trichloride; In chloroform; for 1h; Heating;

DOI:10.1055/s-1996-4382

Reference yield: 55.0%

4,6-Dimethyl-1-oxy-pyridine-3-sulfonic acid p-tolylamide (184433-66-7) → 4,6-Dimethyl-1-oxy-pyridine-3-sulfonic acid (4-methyl-2-nitro-phenyl)-amide

Guidance literature:

With hydrogenchloride; sodium nitrite; In acetonitrile; for 72h; Ambient temperature;

DOI:10.1055/s-1996-4382

upstream raw materials:

3,5-Dimethyl-1,1-dioxo-2-p-tolyl-1,2-dihydro-1λ⁶-[1,2]thiazine-6-carbaldehyde