ethyl 3-((4-bromo-2-fluorophenyl)amino)-3-iminopropanoate hydrochloride

Base Information

Chemical Name:ethyl 3-((4-bromo-2-fluorophenyl)amino)-3-iminopropanoate hydrochloride
CAS No.:1088714-34-4
Molecular Formula:C₁₁H₁₂BrFN₂O₂*ClH
Molecular Weight:339.592
Hs Code.:

Synonyms:ethyl 3-((4-bromo-2-fluorophenyl)amino)-3-iminopropanoate hydrochloride

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Chemical Property of ethyl 3-((4-bromo-2-fluorophenyl)amino)-3-iminopropanoate hydrochloride

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Technology Process of ethyl 3-((4-bromo-2-fluorophenyl)amino)-3-iminopropanoate hydrochloride

There total 1 articles about ethyl 3-((4-bromo-2-fluorophenyl)amino)-3-iminopropanoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 53461-72-6
ethyl 3-imino-3-phenoxypropionate hydrochloride

: 367-24-8
4-bromo-2-fluoroaniline

: 1088714-34-4
ethyl 3-((4-bromo-2-fluorophenyl)amino)-3-iminopropanoate hydrochloride

Guidance literature:: In ethyl acetate; for 2h; Heating / reflux;

Reference yield:

: 1088714-34-4
ethyl 3-((4-bromo-2-fluorophenyl)amino)-3-iminopropanoate hydrochloride

: 1023742-62-2
ethyl 3-((4-bromo-2-fluorophenyl)amino)-3-iminopropanoate

Guidance literature:: With sodium carbonate; In water;

Reference yield:

: 1088714-34-4
ethyl 3-((4-bromo-2-fluorophenyl)amino)-3-iminopropanoate hydrochloride

: 1088714-06-0
ethyl 2-(4-bromo-2-fluorophenylamino)-1-methyl-7-oxo-4,5,6,7-tetrahydro-1H-indole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran / Reflux

1.2: Reflux

2.1: caesium carbonate / N,N-dimethyl-formamide

With sodium hydrogencarbonate; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.02.026