Cyclohexyl-[1-{6-[2,3,4-trimethoxy-6-(2-methyl-[1,3]dithian-2-yl)-phenyl]-benzo[1,3]dioxol-5-yl}-meth-(Z)-ylidene]-amine

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Chemical Name:Cyclohexyl-[1-{6-[2,3,4-trimethoxy-6-(2-methyl-[1,3]dithian-2-yl)-phenyl]-benzo[1,3]dioxol-5-yl}-meth-(Z)-ylidene]-amine
CAS No.:750638-14-3
Molecular Formula:C₂₈H₃₅NO₅S₂
Molecular Weight:529.722
Hs Code.:

Synonyms:Cyclohexyl-[1-{6-[2,3,4-trimethoxy-6-(2-methyl-[1,3]dithian-2-yl)-phenyl]-benzo[1,3]dioxol-5-yl}-meth-(Z)-ylidene]-amine

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Chemical Property of Cyclohexyl-[1-{6-[2,3,4-trimethoxy-6-(2-methyl-[1,3]dithian-2-yl)-phenyl]-benzo[1,3]dioxol-5-yl}-meth-(Z)-ylidene]-amine

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Technology Process of Cyclohexyl-[1-{6-[2,3,4-trimethoxy-6-(2-methyl-[1,3]dithian-2-yl)-phenyl]-benzo[1,3]dioxol-5-yl}-meth-(Z)-ylidene]-amine

There total 5 articles about Cyclohexyl-[1-{6-[2,3,4-trimethoxy-6-(2-methyl-[1,3]dithian-2-yl)-phenyl]-benzo[1,3]dioxol-5-yl}-meth-(Z)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3840-31-1
(3,4,5-trimethoxyphenyl)methanol

: 750638-14-3
Cyclohexyl-[1-{6-[2,3,4-trimethoxy-6-(2-methyl-[1,3]dithian-2-yl)-phenyl]-benzo[1,3]dioxol-5-yl}-meth-(Z)-ylidene]-amine

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / N-bromosuccinimide / CHCl₃ / 3 h / Heating

2: 85 percent / MnO₂ / benzene

3: 4.46 g / diethyl ether / 1 h

4: pyridinium chlorochromate / CH₂Cl₂ / 18 h

5: 96 percent / HCl gas / CHCl₃ / 1.2 h / ice bath

6: 1.) n-BuLi, 2.) CuI*P(OEt)3

With hydrogenchloride; manganese(IV) oxide; N-Bromosuccinimide; n-butyllithium; triethylphosphite copper(I) iodide complex; pyridinium chlorochromate; In diethyl ether; dichloromethane; chloroform; benzene;
DOI:10.1021/ja00522a058

Reference yield:

: 73252-54-7
(2-bromo-3,4,5-trimethoxyphenyl)methanol

: 750638-14-3
Cyclohexyl-[1-{6-[2,3,4-trimethoxy-6-(2-methyl-[1,3]dithian-2-yl)-phenyl]-benzo[1,3]dioxol-5-yl}-meth-(Z)-ylidene]-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / MnO₂ / benzene

2: 4.46 g / diethyl ether / 1 h

3: pyridinium chlorochromate / CH₂Cl₂ / 18 h

4: 96 percent / HCl gas / CHCl₃ / 1.2 h / ice bath

5: 1.) n-BuLi, 2.) CuI*P(OEt)3

With hydrogenchloride; manganese(IV) oxide; n-butyllithium; triethylphosphite copper(I) iodide complex; pyridinium chlorochromate; In diethyl ether; dichloromethane; chloroform; benzene;
DOI:10.1021/ja00522a058

Reference yield:

: 2-bromo-α-methyl-3,4,5-trimethoxybenzyl alcohol

: 750638-14-3
Cyclohexyl-[1-{6-[2,3,4-trimethoxy-6-(2-methyl-[1,3]dithian-2-yl)-phenyl]-benzo[1,3]dioxol-5-yl}-meth-(Z)-ylidene]-amine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium chlorochromate / CH₂Cl₂ / 18 h

2: 96 percent / HCl gas / CHCl₃ / 1.2 h / ice bath

3: 1.) n-BuLi, 2.) CuI*P(OEt)3

With hydrogenchloride; n-butyllithium; triethylphosphite copper(I) iodide complex; pyridinium chlorochromate; In dichloromethane; chloroform;
DOI:10.1021/ja00522a058