(2S,3S)-2-(benzyloxycarbonylamino)-1-methoxy-1,6-dioxooctadecan-3-yl benzoate

Base Information

Chemical Name:(2S,3S)-2-(benzyloxycarbonylamino)-1-methoxy-1,6-dioxooctadecan-3-yl benzoate
CAS No.:952143-98-5
Molecular Formula:C₃₄H₄₇NO₇
Molecular Weight:581.75
Hs Code.:

Synonyms:(2S,3S)-2-(benzyloxycarbonylamino)-1-methoxy-1,6-dioxooctadecan-3-yl benzoate

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Chemical Property of (2S,3S)-2-(benzyloxycarbonylamino)-1-methoxy-1,6-dioxooctadecan-3-yl benzoate

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Technology Process of (2S,3S)-2-(benzyloxycarbonylamino)-1-methoxy-1,6-dioxooctadecan-3-yl benzoate

There total 6 articles about (2S,3S)-2-(benzyloxycarbonylamino)-1-methoxy-1,6-dioxooctadecan-3-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 914618-54-5
(1R,2S)-1,2-bis(benzyloxy)-1-p-methoxyphenylbut-3-ene

: 952143-98-5
(2S,3S)-2-(benzyloxycarbonylamino)-1-methoxy-1,6-dioxooctadecan-3-yl benzoate

Guidance literature:: Multi-step reaction with 6 steps

1: Na₂CO₃ / toluene / 24 h / -78 °C

2: 11.0 g / Na₂SO₃ / ethyl acetate; H₂O / 24 h / 20 °C

3: 88 percent / Hoveyda 2^nd Grubbs catalyst / toluene / 48 h / 80 °C

4: 70 percent / H₂ / PtO₂ / ethyl acetate / 2 h / 20 °C / 3102.97 Torr

5: RuCl₃; NaIO₄ / H₂O; acetonitrile; ethyl acetate / 4 h / 20 °C

6: 3.8 g / diethyl ether / 1 h / 0 °C

With ruthenium trichloride; sodium periodate; hydrogen; sodium carbonate; sodium sulfite; platinum(IV) oxide; In diethyl ether; water; ethyl acetate; toluene; acetonitrile;
DOI:10.1016/j.tetlet.2007.07.034

Reference yield:

: 914618-53-4
(1R,2S)-benzyl N-(2-benzyloxy-1-p-methoxyphenylbut-3-enyl)carbamate

: 952143-98-5
(2S,3S)-2-(benzyloxycarbonylamino)-1-methoxy-1,6-dioxooctadecan-3-yl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / Hoveyda 2^nd Grubbs catalyst / toluene / 48 h / 80 °C

2: 70 percent / H₂ / PtO₂ / ethyl acetate / 2 h / 20 °C / 3102.97 Torr

3: RuCl₃; NaIO₄ / H₂O; acetonitrile; ethyl acetate / 4 h / 20 °C

4: 3.8 g / diethyl ether / 1 h / 0 °C

With ruthenium trichloride; sodium periodate; hydrogen; platinum(IV) oxide; In diethyl ether; water; ethyl acetate; toluene; acetonitrile;
DOI:10.1016/j.tetlet.2007.07.034

Reference yield:

: 952143-96-3
benzyl (1R,2S)-2-(benzyloxy)-1-(4-methoxyphenyl)-5-oxoheptadecen-(3E)-enyl carbamate

: 952143-98-5
(2S,3S)-2-(benzyloxycarbonylamino)-1-methoxy-1,6-dioxooctadecan-3-yl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / H₂ / PtO₂ / ethyl acetate / 2 h / 20 °C / 3102.97 Torr

2: RuCl₃; NaIO₄ / H₂O; acetonitrile; ethyl acetate / 4 h / 20 °C

3: 3.8 g / diethyl ether / 1 h / 0 °C

With ruthenium trichloride; sodium periodate; hydrogen; platinum(IV) oxide; In diethyl ether; water; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetlet.2007.07.034