(2S,3S,6S)-methyl 3-(benzyloxy)-6-dodecylpiperidine-2-carboxylate

Base Information

Chemical Name:(2S,3S,6S)-methyl 3-(benzyloxy)-6-dodecylpiperidine-2-carboxylate
CAS No.:952143-95-2
Molecular Formula:C₂₆H₄₁NO₄
Molecular Weight:431.616
Hs Code.:

Synonyms:(2S,3S,6S)-methyl 3-(benzyloxy)-6-dodecylpiperidine-2-carboxylate

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Chemical Property of (2S,3S,6S)-methyl 3-(benzyloxy)-6-dodecylpiperidine-2-carboxylate

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Technology Process of (2S,3S,6S)-methyl 3-(benzyloxy)-6-dodecylpiperidine-2-carboxylate

There total 7 articles about (2S,3S,6S)-methyl 3-(benzyloxy)-6-dodecylpiperidine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 952143-98-5
(2S,3S)-2-(benzyloxycarbonylamino)-1-methoxy-1,6-dioxooctadecan-3-yl benzoate

: 952143-95-2
(2S,3S,6S)-methyl 3-(benzyloxy)-6-dodecylpiperidine-2-carboxylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 24h; under 3102.97 Torr;
DOI:10.1016/j.tetlet.2007.07.034

Reference yield:

: 914618-54-5
(1R,2S)-1,2-bis(benzyloxy)-1-p-methoxyphenylbut-3-ene

: 952143-95-2
(2S,3S,6S)-methyl 3-(benzyloxy)-6-dodecylpiperidine-2-carboxylate

Guidance literature:: Multi-step reaction with 7 steps

1: Na₂CO₃ / toluene / 24 h / -78 °C

2: 11.0 g / Na₂SO₃ / ethyl acetate; H₂O / 24 h / 20 °C

3: 88 percent / Hoveyda 2^nd Grubbs catalyst / toluene / 48 h / 80 °C

4: 70 percent / H₂ / PtO₂ / ethyl acetate / 2 h / 20 °C / 3102.97 Torr

5: RuCl₃; NaIO₄ / H₂O; acetonitrile; ethyl acetate / 4 h / 20 °C

6: 3.8 g / diethyl ether / 1 h / 0 °C

7: 83 percent / H₂ / Pd/C / methanol / 24 h / 20 °C / 3102.97 Torr

With ruthenium trichloride; sodium periodate; hydrogen; sodium carbonate; sodium sulfite; platinum(IV) oxide; palladium on activated charcoal; In methanol; diethyl ether; water; ethyl acetate; toluene; acetonitrile;
DOI:10.1016/j.tetlet.2007.07.034

Reference yield:

: 914618-53-4
(1R,2S)-benzyl N-(2-benzyloxy-1-p-methoxyphenylbut-3-enyl)carbamate

: 952143-95-2
(2S,3S,6S)-methyl 3-(benzyloxy)-6-dodecylpiperidine-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / Hoveyda 2^nd Grubbs catalyst / toluene / 48 h / 80 °C

2: 70 percent / H₂ / PtO₂ / ethyl acetate / 2 h / 20 °C / 3102.97 Torr

3: RuCl₃; NaIO₄ / H₂O; acetonitrile; ethyl acetate / 4 h / 20 °C

4: 3.8 g / diethyl ether / 1 h / 0 °C

5: 83 percent / H₂ / Pd/C / methanol / 24 h / 20 °C / 3102.97 Torr

With ruthenium trichloride; sodium periodate; hydrogen; platinum(IV) oxide; palladium on activated charcoal; In methanol; diethyl ether; water; ethyl acetate; toluene; acetonitrile;
DOI:10.1016/j.tetlet.2007.07.034