methyl (2S)-[(3-amino-2-naphthoyl)amino](cyclohexyl)ethanoate hydrochloride

Base Information

• Chemical Name: methyl (2S)-[(3-amino-2-naphthoyl)amino](cyclohexyl)ethanoate hydrochloride
• CAS No.: 887242-61-7
• Molecular Formula: C₂₀H₂₄N₂O₃*ClH
• Molecular Weight: 376.883

Synonyms:methyl (2S)-[(3-amino-2-naphthoyl)amino](cyclohexyl)ethanoate hydrochloride

Chemical Property of methyl (2S)-[(3-amino-2-naphthoyl)amino](cyclohexyl)ethanoate hydrochloride

Chemical Property:

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Technology Process of methyl (2S)-[(3-amino-2-naphthoyl)amino](cyclohexyl)ethanoate hydrochloride

There total 1 articles about methyl (2S)-[(3-amino-2-naphthoyl)amino](cyclohexyl)ethanoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl (2S)-({3-[(tert-butoxycarbonyl)amino]-2-naphthoyl}amino)(cyclohexyl)ethanoate (887242-60-6) → methyl (2S)-[(3-amino-2-naphthoyl)amino](cyclohexyl)ethanoate hydrochloride (887242-61-7)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1.5h;

Reference yield:

[2,6-dichloro-4-(trifluoromethyl) phenyl] acetic acid (132992-36-0) + methyl (2S)-[(3-amino-2-naphthoyl)amino](cyclohexyl)ethanoate hydrochloride (887242-61-7) → methyl (2S)-cyclohexyl{[3-({[2,6-dichloro-4-(trifluoromethyl)phenyl]acetyl}amino)-2-naphthoyl]amino}ethanoate (887242-63-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

Reference yield:

methyl (2S)-[(3-amino-2-naphthoyl)amino](cyclohexyl)ethanoate hydrochloride (887242-61-7) + 2,4,6-trichlorophenyl isocyanate (2505-31-9) → methyl (2S)-cyclohexyl{[3-({[(2,4,6-trichlorophenyl)amino]carbonyl}amino)-2-naphthoyl]amino}ethanoate (887242-62-8)

Guidance literature:

With pyridine; at 20 ℃; for 4h;

upstream raw materials:

methyl (2S)-({3-[(tert-butoxycarbonyl)amino]-2-naphthoyl}amino)(cyclohexyl)ethanoate

Downstream raw materials:

methyl (2S)-cyclohexyl{[3-({[(2,4,6-trichlorophenyl)amino]carbonyl}amino)-2-naphthoyl]amino}ethanoate

methyl (2S)-cyclohexyl{[3-({[2,6-dichloro-4-(trifluoromethyl)phenyl]acetyl}amino)-2-naphthoyl]amino}ethanoate

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