2-methyl-12-phenyl-4b,6-dihydrobenzo[4,5][1,3]oxazino[2,3-a]isoquinoline

Base Information

Chemical Name:2-methyl-12-phenyl-4b,6-dihydrobenzo[4,5][1,3]oxazino[2,3-a]isoquinoline
CAS No.:1428747-64-1
Molecular Formula:C₂₃H₁₉NO
Molecular Weight:325.41
Hs Code.:

Synonyms:2-methyl-12-phenyl-4b,6-dihydrobenzo[4,5][1,3]oxazino[2,3-a]isoquinoline

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Chemical Property of 2-methyl-12-phenyl-4b,6-dihydrobenzo[4,5][1,3]oxazino[2,3-a]isoquinoline

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Technology Process of 2-methyl-12-phenyl-4b,6-dihydrobenzo[4,5][1,3]oxazino[2,3-a]isoquinoline

There total 3 articles about 2-methyl-12-phenyl-4b,6-dihydrobenzo[4,5][1,3]oxazino[2,3-a]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5344-90-1
2-Aminobenzyl alcohol

: 1034421-82-3
2-(2-phenylethynyl)-4-methylbenzaldehyde

: 1428747-64-1
2-methyl-12-phenyl-4b,6-dihydrobenzo[4,5][1,3]oxazino[2,3-a]isoquinoline

Guidance literature:: With silver nitrate; In toluene; at 80 ℃; for 3h; Sealed tube;
DOI:10.3390/molecules18010814

Reference yield:

: 824-54-4
2-bromo-4-methylbenzaldehyde

: 1428747-64-1
2-methyl-12-phenyl-4b,6-dihydrobenzo[4,5][1,3]oxazino[2,3-a]isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 4 h / 60 °C / Inert atmosphere

2: silver nitrate / toluene / 3 h / 80 °C / Sealed tube

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; silver nitrate; triethylamine; In toluene;
DOI:10.3390/molecules18010814

Reference yield:

: 536-74-3
phenylacetylene

: 1428747-64-1
2-methyl-12-phenyl-4b,6-dihydrobenzo[4,5][1,3]oxazino[2,3-a]isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 4 h / 60 °C / Inert atmosphere

2: silver nitrate / toluene / 3 h / 80 °C / Sealed tube

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; silver nitrate; triethylamine; In toluene;
DOI:10.3390/molecules18010814