(RS)-methyl 2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)-propanoate

Base Information

Chemical Name:(RS)-methyl 2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)-propanoate
CAS No.:1370228-78-6
Molecular Formula:C₂₂H₂₈N₂O₇S
Molecular Weight:464.54
Hs Code.:

Synonyms:(RS)-methyl 2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)-propanoate

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Chemical Property of (RS)-methyl 2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)-propanoate

Chemical Property:

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Technology Process of (RS)-methyl 2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)-propanoate

There total 1 articles about (RS)-methyl 2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)-propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1370228-74-2
(RS)-methyl 2-((N-(tert-butoxycarbonyl)sulfamoyl)amino)propanoate

: 13826-35-2
3-Phenoxybenzyl alcohol

: 1370228-78-6
(RS)-methyl 2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)-propanoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1016/j.bmc.2012.01.030

Reference yield: 71.0%

: 1370228-78-6
(RS)-methyl 2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)-propanoate

: 1370228-83-3
(RS)-2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)propanoic acid

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.bmc.2012.01.030

Reference yield: 22.0%

: 1370228-78-6
(RS)-methyl 2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)-propanoate

: 100-39-0
benzyl bromide

: 1370228-98-0
methyl 2-(benzyl(N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)acetate

Guidance literature:: (RS)-methyl 2-((N-(tert-butoxycarbonyl)-N-(3-phenoxybenzyl)sulfamoyl)amino)-propanoate; With sodium hydride; In acetonitrile;

benzyl bromide; In acetonitrile;
DOI:10.1016/j.bmc.2012.01.030