C₃₉H₇₇IO₅Si₃

Base Information

Chemical Name:C₃₉H₇₇IO₅Si₃
CAS No.:902131-93-5
Molecular Formula:C₃₉H₇₇IO₅Si₃
Molecular Weight:837.198
Hs Code.:

C<sub>39</sub>H<sub>77</sub>IO<sub>5</sub>Si<sub>3</sub>

Synonyms:C₃₉H₇₇IO₅Si₃

Suppliers and Price of C₃₉H₇₇IO₅Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₉H₇₇IO₅Si₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₉H₇₇IO₅Si₃

There total 16 articles about C₃₉H₇₇IO₅Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 902131-92-4
C₃₉H₇₈O₆Si₃

: 902131-93-5
C₃₉H₇₇IO₅Si₃

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In benzene; at 0 - 25 ℃; for 0.5h;
DOI:10.1039/b602020h

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 902131-93-5
C₃₉H₇₇IO₅Si₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: 89 percent / imidazole; 4-DMAP / CH₂Cl₂ / 7 h / 20 °C

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: 92 percent / PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

3.1: diethyl ether; tetrahydrofuran / 3 h / -78 °C

3.2: 59.79 g / aq. NaOH; H₂O₂ / tetrahydrofuran; diethyl ether / 16 h / 0 - 25 °C

4.1: 95 percent / imidazole; 4-DMAP / CH₂Cl₂ / 7 h / 20 °C

5.1: O₃ / CH₂Cl₂ / -78 °C

5.2: 90 percent / PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

6.1: 98 percent / NaBH₄ / methanol / 0.17 h / 0 °C

7.1: 98 percent / PPh₃; I₂; imidazole / benzene / 0.5 h / 0 - 25 °C

With 1H-imidazole; dmap; sodium tetrahydroborate; iodine; ozone; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene; 3.1: Brown allylation;
DOI:10.1039/b602020h

Reference yield:

: 902131-79-7
C₃₃H₃₆O₃

: 902131-93-5
C₃₉H₇₇IO₅Si₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: 90 percent / TsOH*H₂O / methanol / 0.33 h / 25 °C

2.1: 99 percent / (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 1 h / -78 - 25 °C

3.1: 99 percent / MgBr₂ / diethyl ether / 3 h / 0 °C

4.1: 95 percent / imidazole; 4-DMAP / CH₂Cl₂ / 16 h / 20 °C

5.1: BH₃*SMe₂ / tetrahydrofuran / 7 h / 0 - 25 °C

5.2: 85 percent / aq. NaOH; H₂O₂ / tetrahydrofuran; diethyl ether / 16 h / 0 - 25 °C

6.1: 93 percent / (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 1 h / -78 - 25 °C

7.1: diethyl ether; tetrahydrofuran / 3 h / -78 °C

7.2: 62.3 g / aq. NaOH; H₂O₂ / tetrahydrofuran; diethyl ether / 16 h / 0 - 25 °C

8.1: 89 percent / imidazole; 4-DMAP / CH₂Cl₂ / 7 h / 20 °C

9.1: O₃ / CH₂Cl₂ / -78 °C

9.2: 92 percent / PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

10.1: diethyl ether; tetrahydrofuran / 3 h / -78 °C

10.2: 59.79 g / aq. NaOH; H₂O₂ / tetrahydrofuran; diethyl ether / 16 h / 0 - 25 °C

11.1: 95 percent / imidazole; 4-DMAP / CH₂Cl₂ / 7 h / 20 °C

12.1: O₃ / CH₂Cl₂ / -78 °C

12.2: 90 percent / PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

13.1: 98 percent / NaBH₄ / methanol / 0.17 h / 0 °C

14.1: 98 percent / PPh₃; I₂; imidazole / benzene / 0.5 h / 0 - 25 °C

With 1H-imidazole; dmap; sodium tetrahydroborate; oxalyl dichloride; dimethylsulfide borane complex; iodine; toluene-4-sulfonic acid; ozone; dimethyl sulfoxide; triethylamine; triphenylphosphine; magnesium bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene; 2.1: Swern oxidation / 6.1: Swern oxidation / 7.1: Brown allylation / 10.1: Brown allylation;
DOI:10.1039/b602020h