(Z)-4-((1-(2-(benzyloxy)-4-nitrophenyl)-5-methyl-1-oxohex-2-en-3-yl)amino)-2-methoxybenzamide

Base Information

Chemical Name:(Z)-4-((1-(2-(benzyloxy)-4-nitrophenyl)-5-methyl-1-oxohex-2-en-3-yl)amino)-2-methoxybenzamide
CAS No.:1319746-28-5
Molecular Formula:C₂₈H₂₉N₃O₆
Molecular Weight:503.555
Hs Code.:

Synonyms:(Z)-4-((1-(2-(benzyloxy)-4-nitrophenyl)-5-methyl-1-oxohex-2-en-3-yl)amino)-2-methoxybenzamide

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Chemical Property of (Z)-4-((1-(2-(benzyloxy)-4-nitrophenyl)-5-methyl-1-oxohex-2-en-3-yl)amino)-2-methoxybenzamide

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Technology Process of (Z)-4-((1-(2-(benzyloxy)-4-nitrophenyl)-5-methyl-1-oxohex-2-en-3-yl)amino)-2-methoxybenzamide

There total 10 articles about (Z)-4-((1-(2-(benzyloxy)-4-nitrophenyl)-5-methyl-1-oxohex-2-en-3-yl)amino)-2-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 1319746-21-8
1-(2-(benzyloxy)-4-nitrophenyl)-5-methylhex-2-yn-1-one

: 75955-30-5
4-amino-2-methoxybenzamide

: 1319746-28-5
(Z)-4-((1-(2-(benzyloxy)-4-nitrophenyl)-5-methyl-1-oxohex-2-en-3-yl)amino)-2-methoxybenzamide

Guidance literature:: In methanol; at 120 ℃; for 3h;
DOI:10.1021/jo200917d

Reference yield:

: 619-19-2
2-hydroxy-4-nitrobenzoic acid

: 1319746-28-5
(Z)-4-((1-(2-(benzyloxy)-4-nitrophenyl)-5-methyl-1-oxohex-2-en-3-yl)amino)-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 80 °C / Inert atmosphere

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: ammonium hydroxide / dichloromethane / Inert atmosphere

4: platinum(IV) oxide; hydrogen; potassium carbonate / methanol / 0.75 h

5: methanol / 3 h / 120 °C

With platinum(IV) oxide; ammonium hydroxide; oxalyl dichloride; hydrogen; potassium carbonate; N,N-dimethyl-formamide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo200917d

Reference yield:

: 39787-83-2
2-methoxy-4-nitrobenzoyl chloride

: 1319746-28-5
(Z)-4-((1-(2-(benzyloxy)-4-nitrophenyl)-5-methyl-1-oxohex-2-en-3-yl)amino)-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium hydroxide / dichloromethane / Inert atmosphere

2: platinum(IV) oxide; hydrogen; potassium carbonate / methanol / 0.75 h

3: methanol / 3 h / 120 °C

With platinum(IV) oxide; ammonium hydroxide; hydrogen; potassium carbonate; In methanol; dichloromethane;
DOI:10.1021/jo200917d