methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-6-O-triphenylmethyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-6-O-triphenylmethyl-α-D-glucopyranoside
CAS No.:155630-85-6
Molecular Formula:C₆₉H₆₉NO₁₄
Molecular Weight:1136.31
Hs Code.:

methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-6-O-triphenylmethyl-α-D-glucopyranoside

Synonyms:methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-6-O-triphenylmethyl-α-D-glucopyranoside

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Chemical Property of methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-6-O-triphenylmethyl-α-D-glucopyranoside

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Technology Process of methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-6-O-triphenylmethyl-α-D-glucopyranoside

There total 6 articles about methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-6-O-triphenylmethyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 76-83-5
trityl chloride

: 155630-84-5
methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

: 155630-85-6
methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-6-O-triphenylmethyl-α-D-glucopyranoside

Guidance literature:: With triethylamine; In dichloromethane; toluene; at 110 ℃;
DOI:10.1016/S0008-6215(00)90986-8

Reference yield:

: 100-39-0
benzyl bromide

: 155630-85-6
methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-6-O-triphenylmethyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / KHCO₃ / dimethylformamide / 15 h / 20 °C

2: 95 percent / triethylamine / CH₂Cl₂; toluene / 110 °C

With potassium hydrogencarbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0008-6215(00)90986-8

Reference yield:

: 4-methoxyphenyl 2,2,2-trichloroacetimidate

: 155630-85-6
methyl 3-O-benzyl-4-O-(benzyl 3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-2-benzyloxycarbonylamino-2-deoxy-6-O-triphenylmethyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / trifluoromethanesulphonic acid / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

2: 92 percent / 4M aq. NaOH / CH₂Cl₂; methanol / 2 h / 20 °C

3: 85 percent / KHCO₃ / dimethylformamide / 15 h / 20 °C

4: 95 percent / triethylamine / CH₂Cl₂; toluene / 110 °C

With sodium hydroxide; trifluorormethanesulfonic acid; potassium hydrogencarbonate; triethylamine; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0008-6215(00)90986-8