4-benzyl 1-ethyl 2-chloroterephthalate

Base Information

Chemical Name:4-benzyl 1-ethyl 2-chloroterephthalate
CAS No.:911313-98-9
Molecular Formula:C₁₇H₁₅ClO₄
Molecular Weight:318.757
Hs Code.:

Synonyms:4-benzyl 1-ethyl 2-chloroterephthalate

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Chemical Property of 4-benzyl 1-ethyl 2-chloroterephthalate

Chemical Property:

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Technology Process of 4-benzyl 1-ethyl 2-chloroterephthalate

There total 1 articles about 4-benzyl 1-ethyl 2-chloroterephthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76008-74-7
Ethyl 4-bromo-2-chlorobenzoate

: 201230-82-2
carbon monoxide

: 100-51-6,185532-71-2
benzyl alcohol

: 911313-98-9
4-benzyl 1-ethyl 2-chloroterephthalate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane; In dimethyl sulfoxide; at 100 ℃; for 9h;

Reference yield:

: 911313-98-9
4-benzyl 1-ethyl 2-chloroterephthalate

: 911314-33-5
1-ethyl 2-chloroterephthalate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: 911313-98-9
4-benzyl 1-ethyl 2-chloroterephthalate

: 911313-99-0
Ethyl 2-chloro-4-(2-hydroxy-1-methylethyl)aminocarbonylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 3 h / 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 96 h / 20 °C

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In tetrahydrofuran; N,N-dimethyl-formamide;