(+/-)-β-(3-methoxy-2,4,6-trimethylphenyl)-N,N-dimethyl-1,3-dioxolane-2-butanamine

Base Information

Chemical Name:(+/-)-β-(3-methoxy-2,4,6-trimethylphenyl)-N,N-dimethyl-1,3-dioxolane-2-butanamine
CAS No.:318294-48-3
Molecular Formula:C₁₉H₃₁NO₃
Molecular Weight:321.46
Hs Code.:

Synonyms:(+/-)-β-(3-methoxy-2,4,6-trimethylphenyl)-N,N-dimethyl-1,3-dioxolane-2-butanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-β-(3-methoxy-2,4,6-trimethylphenyl)-N,N-dimethyl-1,3-dioxolane-2-butanamine

Chemical Property:

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Technology Process of (+/-)-β-(3-methoxy-2,4,6-trimethylphenyl)-N,N-dimethyl-1,3-dioxolane-2-butanamine

There total 1 articles about (+/-)-β-(3-methoxy-2,4,6-trimethylphenyl)-N,N-dimethyl-1,3-dioxolane-2-butanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 318294-47-2
(+/-)-β-(3-methoxy-2,4,6-trimethylphenyl)-1,3-dioxolane-2-butanamine

: 318294-48-3
(+/-)-β-(3-methoxy-2,4,6-trimethylphenyl)-N,N-dimethyl-1,3-dioxolane-2-butanamine

Guidance literature:: With sodium cyanoborohydride; zinc(II) chloride; In methanol; at 20 ℃; for 10h;
DOI:10.1002/1522-2675(20000906)83:9<2246::AID-HLCA2246>3.0.CO;2-X

Reference yield: 100.0%

: 318294-48-3
(+/-)-β-(3-methoxy-2,4,6-trimethylphenyl)-N,N-dimethyl-1,3-dioxolane-2-butanamine

: 318294-49-4
(+/-)-γ-[(dimethylamino)methyl]-3-methoxy-2,4,6-trimethylbenzenebutanal

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1002/1522-2675(20000906)83:9<2246::AID-HLCA2246>3.0.CO;2-X

Reference yield:

: 318294-48-3
(+/-)-β-(3-methoxy-2,4,6-trimethylphenyl)-N,N-dimethyl-1,3-dioxolane-2-butanamine

: (+/-)-4-(3-methoxy-2,4,6-trimethylphenyl)-2-methylpenta-2,4-dienal

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 3N HCl / tetrahydrofuran / 24 h / 20 °C

2: 98 percent / Me₂N*HCl (Eschenmoser salt) / tetrahydrofuran / 3 h / Heating

3: 4.2 mg / AlCl₃ / CHCl₃ / 12 h / -78 °C

With hydrogenchloride; aluminium trichloride; N,N-dimethyl(methylene)ammonium chloride; In tetrahydrofuran; chloroform; 1: Hydrolysis / 2: Condensation / 3: Elimination;
DOI:10.1002/1522-2675(20000906)83:9<2246::AID-HLCA2246>3.0.CO;2-X