4-{N-benzyl-N-[3-(methylselanyl)-3-oxopropyl]aminocyclohex}-1-enecarbonitrile

Base Information

Chemical Name:4-{N-benzyl-N-[3-(methylselanyl)-3-oxopropyl]aminocyclohex}-1-enecarbonitrile
CAS No.:187807-27-8
Molecular Formula:C₁₈H₂₂N₂OSe
Molecular Weight:361.345
Hs Code.:

Synonyms:4-{N-benzyl-N-[3-(methylselanyl)-3-oxopropyl]aminocyclohex}-1-enecarbonitrile

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Chemical Property of 4-{N-benzyl-N-[3-(methylselanyl)-3-oxopropyl]aminocyclohex}-1-enecarbonitrile

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Technology Process of 4-{N-benzyl-N-[3-(methylselanyl)-3-oxopropyl]aminocyclohex}-1-enecarbonitrile

There total 6 articles about 4-{N-benzyl-N-[3-(methylselanyl)-3-oxopropyl]aminocyclohex}-1-enecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 67132-62-1
dimethyl aluminum selenide

: 422507-26-4
4-[N-benzyl-N-(2-methoxycarbonylethyl)amino]-1-cyclohexenecarbonitrile

: methylselanyl 3-methylselanylpropionate

: 187807-27-8
4-{N-benzyl-N-[3-(methylselanyl)-3-oxopropyl]aminocyclohex}-1-enecarbonitrile

Guidance literature:: In dichloromethane; toluene; at 0 - 20 ℃; for 9h;
DOI:10.1021/jo0163849

Reference yield:

: 142009-99-2
4-(benzylamino)cyclohexane-1-one

: 187807-27-8
4-{N-benzyl-N-[3-(methylselanyl)-3-oxopropyl]aminocyclohex}-1-enecarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: ZnI₂

1.2: POCl₃

1.3: 50 percent / aq. HCl / tetrahydrofuran

2.1: 20 percent / ethanol / 24 h / Heating

3.1: 23 percent / CH₂Cl₂; toluene / 9 h / 0 - 20 °C

With zinc(II) iodide; In ethanol; dichloromethane; toluene;
DOI:10.1021/jo0163849

Reference yield:

: 422507-45-7
4-benzylamino-1-trimethylsilyloxycyclohexane-1-carbonitrile

: 187807-27-8
4-{N-benzyl-N-[3-(methylselanyl)-3-oxopropyl]aminocyclohex}-1-enecarbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / pyridine; POCl₃ / benzene / 5 h / Heating

2: 87 percent / aq. HCl / tetrahydrofuran / 5 h / Heating

3: 20 percent / ethanol / 24 h / Heating

4: 23 percent / CH₂Cl₂; toluene / 9 h / 0 - 20 °C

With pyridine; hydrogenchloride; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane; toluene; benzene;
DOI:10.1021/jo0163849