6-amino-1-methyl-5-[3-phenyl-(E,2E)-2-propenylidenamino]-1,2,3,4-tetrahydro-2,4-pyrimidindione

Base Information

Chemical Name:6-amino-1-methyl-5-[3-phenyl-(E,2E)-2-propenylidenamino]-1,2,3,4-tetrahydro-2,4-pyrimidindione
CAS No.:343362-39-0
Molecular Formula:C₁₄H₁₄N₄O₂
Molecular Weight:270.291
Hs Code.:

Synonyms:6-amino-1-methyl-5-[3-phenyl-(E,2E)-2-propenylidenamino]-1,2,3,4-tetrahydro-2,4-pyrimidindione

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Chemical Property of 6-amino-1-methyl-5-[3-phenyl-(E,2E)-2-propenylidenamino]-1,2,3,4-tetrahydro-2,4-pyrimidindione

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Technology Process of 6-amino-1-methyl-5-[3-phenyl-(E,2E)-2-propenylidenamino]-1,2,3,4-tetrahydro-2,4-pyrimidindione

There total 3 articles about 6-amino-1-methyl-5-[3-phenyl-(E,2E)-2-propenylidenamino]-1,2,3,4-tetrahydro-2,4-pyrimidindione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 6972-82-3
5,6-diamino-1-methyluracil

: 343362-39-0
6-amino-1-methyl-5-[3-phenyl-(E,2E)-2-propenylidenamino]-1,2,3,4-tetrahydro-2,4-pyrimidindione

Guidance literature:: With acetic acid; In methanol; at 20 ℃; for 1h;
DOI:10.1021/jm011093d

Reference yield:

: 2434-53-9
6-amino-1-methyluracil

: 343362-39-0
6-amino-1-methyl-5-[3-phenyl-(E,2E)-2-propenylidenamino]-1,2,3,4-tetrahydro-2,4-pyrimidindione

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / aq. NaNO₂; AcOH / 1 h / 20 °C

2: aq. NH₃; Na₂S₂O₄

3: AcOH / methanol / 1 h / 20 °C

With ammonium hydroxide; sodium dithionite; acetic acid; sodium nitrite; In methanol;
DOI:10.1021/jm011093d

Reference yield:

: 6972-78-7
6-amino-1-methyl-5-nitrosouracil

: 343362-39-0
6-amino-1-methyl-5-[3-phenyl-(E,2E)-2-propenylidenamino]-1,2,3,4-tetrahydro-2,4-pyrimidindione

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NH₃; Na₂S₂O₄

2: AcOH / methanol / 1 h / 20 °C

With ammonium hydroxide; sodium dithionite; acetic acid; In methanol;
DOI:10.1021/jm011093d