4-(cyclohexylimino)-3,3,5,5-tetramethyl-3,5-dihydro-4H-pyrazole

Base Information

Chemical Name:4-(cyclohexylimino)-3,3,5,5-tetramethyl-3,5-dihydro-4H-pyrazole
CAS No.:72453-29-3
Molecular Formula:C₁₃H₂₃N₃
Molecular Weight:221.346
Hs Code.:

Synonyms:4-(cyclohexylimino)-3,3,5,5-tetramethyl-3,5-dihydro-4H-pyrazole

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Chemical Property of 4-(cyclohexylimino)-3,3,5,5-tetramethyl-3,5-dihydro-4H-pyrazole

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Technology Process of 4-(cyclohexylimino)-3,3,5,5-tetramethyl-3,5-dihydro-4H-pyrazole

There total 3 articles about 4-(cyclohexylimino)-3,3,5,5-tetramethyl-3,5-dihydro-4H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 108-91-8,157973-60-9
cyclohexylamine

: 30467-62-0
3,3,5,5-tetramethyl-3,5-dihydro-4H-pyrazol-4-one

: 72453-29-3
4-(cyclohexylimino)-3,3,5,5-tetramethyl-3,5-dihydro-4H-pyrazole

Guidance literature:: With Al₂O₃ catalyst (BASF-Katalysator D 10-10); silica gel; at 150 ℃; for 95h;

Reference yield:

: 17346-16-6
2,4-dibromo-2,4-dimethylpentan-3-one

: 72453-29-3
4-(cyclohexylimino)-3,3,5,5-tetramethyl-3,5-dihydro-4H-pyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / NH₂NH₂ hydrate, ethylenediaminetetraacetic acid / ethanol / 3 h / Heating

2: 92 percent / MnO₂-C / various solvent(s) / 30 h / Heating

3: 70 percent / Al₂O₃/SiO₂ crack catalyst, molecular sieves (3 Angstroem) / 120 h / 150 °C

With aluminum oxide; ethylenediaminetetraacetic acid; MnO₂ on activated carbon; 3 A molecular sieve; silica gel; hydrazine hydrate; In ethanol;

Reference yield:

: 55790-79-9
3,3,5,5-tetramethyl-2,3,4,5-tetrahydro-1H-pyrazol-4-one

: 72453-29-3
4-(cyclohexylimino)-3,3,5,5-tetramethyl-3,5-dihydro-4H-pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / MnO₂-C / various solvent(s) / 30 h / Heating

2: 70 percent / Al₂O₃/SiO₂ crack catalyst, molecular sieves (3 Angstroem) / 120 h / 150 °C

With aluminum oxide; MnO₂ on activated carbon; 3 A molecular sieve; silica gel; In various solvent(s);