N¹-{2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-N¹-methyl-heptane-1,7-diamine

Base Information

Chemical Name:N¹-{2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-N¹-methyl-heptane-1,7-diamine
CAS No.:175692-26-9
Molecular Formula:C₂₃H₃₃ClN₂O
Molecular Weight:388.981
Hs Code.:

N<sup>1</sup>-{2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-N<sup>1</sup>-methyl-heptane-1,7-diamine

Synonyms:N¹-{2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-N¹-methyl-heptane-1,7-diamine

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Chemical Property of N¹-{2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-N¹-methyl-heptane-1,7-diamine

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Technology Process of N¹-{2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-N¹-methyl-heptane-1,7-diamine

There total 6 articles about N¹-{2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-N¹-methyl-heptane-1,7-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 175692-20-3
7-({2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-methyl-amino)-heptanenitrile

: 175692-26-9
N¹-{2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-N¹-methyl-heptane-1,7-diamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; for 2h; Ambient temperature;
DOI:10.1002/ardp.19963290206

Reference yield:

: 20965-27-9
7-bromo-heptanonitrile

: 175692-26-9
N¹-{2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-N¹-methyl-heptane-1,7-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / K₂CO₃ / acetonitrile / 90 °C

2: 55 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 2 h / Ambient temperature

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1002/ardp.19963290206

Reference yield:

: 119-56-2
(4-chlorophenyl)phenylmethanol

: 175692-26-9
N¹-{2-[(4-Chloro-phenyl)-phenyl-methoxy]-ethyl}-N¹-methyl-heptane-1,7-diamine

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / NaH / toluene / 5 h / Heating

2: Na₂CO₃ / 1,2-dichloro-ethane / 1) 0 deg C, 10 min, 2) reflux, 2 h

3: 1) CH₃OH, 2) NaOH / 1) r.t., 50 deg C, 2 h, 2) water

4: 84 percent / K₂CO₃ / acetonitrile / 90 °C

5: 55 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 2 h / Ambient temperature

With methanol; sodium hydroxide; lithium aluminium tetrahydride; sodium hydride; sodium carbonate; potassium carbonate; In tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane; toluene; acetonitrile;
DOI:10.1002/ardp.19963290206