N-(2-(4-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)phenyl)methylsulfonamide

Base Information

Chemical Name:N-(2-(4-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)phenyl)methylsulfonamide
CAS No.:1448791-27-2
Molecular Formula:C₁₉H₂₂N₆O₅S
Molecular Weight:446.487
Hs Code.:

Synonyms:N-(2-(4-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)phenyl)methylsulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-(4-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)phenyl)methylsulfonamide

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Technology Process of N-(2-(4-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)phenyl)methylsulfonamide

There total 4 articles about N-(2-(4-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)phenyl)methylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1448791-08-9
N-(2-(4-chloro-6-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)phenyl)methylsulfonamide

: 1448791-27-2
N-(2-(4-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)phenyl)methylsulfonamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; methanol; Inert atmosphere;
DOI:10.1016/j.bmcl.2013.06.038

Reference yield:

: 24313-88-0
3,4,5-Trimethoxyaniline

: 1448791-27-2
N-(2-(4-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)phenyl)methylsulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / -10 °C

2: tetrahydrofuran / 20 °C

3: palladium 10% on activated carbon; triethylamine; hydrogen / tetrahydrofuran; methanol / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2013.06.038

Reference yield:

: 37073-18-0
N-(2-aminophenyl)methanesulfonamide

: 1448791-27-2
N-(2-(4-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)phenyl)methylsulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 20 °C

2: palladium 10% on activated carbon; triethylamine; hydrogen / tetrahydrofuran; methanol / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2013.06.038