trans-Zimtaldehydhydrazon

Base Information

• Chemical Name: trans-Zimtaldehydhydrazon
• CAS No.: 52372-79-9
• Molecular Formula: C₉H₁₀N₂
• Molecular Weight: 146.192
• Mol file: 52372-79-9.mol

Synonyms:trans-Zimtaldehydhydrazon

Chemical Property of trans-Zimtaldehydhydrazon

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of trans-Zimtaldehydhydrazon

There total 3 articles about trans-Zimtaldehydhydrazon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-phenyl-propenal (104-55-2) → 3-phenylallylidenehydrazine (52372-79-9)

Guidance literature:

Multi-step reaction with 2 steps

1: BF₃*Et₂O / ethanol / 3 h / Heating

2: morpholine / 0.75 h / Ambient temperature

With morpholine; boron trifluoride diethyl etherate; In ethanol;

DOI:10.1055/s-1980-28986

Reference yield:

(E)-3-phenylpropenal (14371-10-9) → trans-Zimtaldehydhydrazon (52372-79-9)

Guidance literature:

With hydrazine; In tetrahydrofuran; at 20 ℃; Flow reactor;

DOI:10.1039/c5ob00019j

Reference yield:

N'-[(E)-3-Phenyl-prop-2-en-(E)-ylidene]-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester (74105-58-1) → 3-phenylallylidenehydrazine (52372-79-9)

Guidance literature:

With morpholine; for 0.75h; Yield given; Ambient temperature;

DOI:10.1055/s-1980-28986

upstream raw materials:

(E)-3-phenylpropenal

N'-[(E)-3-Phenyl-prop-2-en-(E)-ylidene]-hydrazinecarboxylic acid 9H-fluoren-9-ylmethyl ester

3-phenyl-propenal

Downstream raw materials:

(E)-(3-diazoprop-1-en-1-yl)benzene

3-phenyl-1,5-hexadiene

(E)-1-phenyl-1,5-hexadiene

1,3-diphenylpropene