(1S,2S)-diethyl cyclohex-4-ene-1,2-diethanoate

Base Information

Chemical Name:(1S,2S)-diethyl cyclohex-4-ene-1,2-diethanoate
CAS No.:173658-53-2
Molecular Formula:C₁₄H₂₂O₄
Molecular Weight:254.326
Hs Code.:

Synonyms:(1S,2S)-diethyl cyclohex-4-ene-1,2-diethanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S)-diethyl cyclohex-4-ene-1,2-diethanoate

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Technology Process of (1S,2S)-diethyl cyclohex-4-ene-1,2-diethanoate

There total 4 articles about (1S,2S)-diethyl cyclohex-4-ene-1,2-diethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 64-17-5
ethanol

: 158250-06-7
(1S,2S)-cyclohex-4-ene-1,2-diethanoic acid

: 173658-53-2
(1S,2S)-diethyl cyclohex-4-ene-1,2-diethanoate

Guidance literature:: With sulfuric acid; for 21h; Heating;
DOI:10.1021/jo951647i

Reference yield:

: 173658-52-1
(1S,2S)-cyclohex-4-ene-1,2-diacetonitrile

: 173658-53-2
(1S,2S)-diethyl cyclohex-4-ene-1,2-diethanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / KOH / ethane-1,2-diol / 5 h / 150 °C

2: 98 percent / conc. H₂SO₄ / 21 h / Heating

With potassium hydroxide; sulfuric acid; In ethylene glycol;
DOI:10.1021/jo951647i

Reference yield:

: 15679-28-4
((1R,6R)-6-(hydroxymethyl)cyclohex-3-enyl)methanol

: 173658-53-2
(1S,2S)-diethyl cyclohex-4-ene-1,2-diethanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / Et₃N / diethyl ether / 1) 0 deg C, 30 min; 2) rt, 24 h

2: 99 percent / dimethylsulfoxide / 4 h / 95 °C

3: 92 percent / KOH / ethane-1,2-diol / 5 h / 150 °C

4: 98 percent / conc. H₂SO₄ / 21 h / Heating

With potassium hydroxide; sulfuric acid; triethylamine; In diethyl ether; ethylene glycol; dimethyl sulfoxide;
DOI:10.1021/jo951647i