7-methoxy-2,3,4,9-tetrahydro-1H-beta-carbolin-1-one

Base Information

• Chemical Name: 7-methoxy-2,3,4,9-tetrahydro-1H-beta-carbolin-1-one
• CAS No.: 26579-69-1
• Molecular Formula: C12H12 N2 O2
• Molecular Weight: 216.239

Synonyms:1,2,3,4-Tetrahydro-7-methoxy-1-oxo-b-carboline; Harmalacidine;Ketotetrahydronorharmine; Oxotetrahydronorharmine

Chemical Property of 7-methoxy-2,3,4,9-tetrahydro-1H-beta-carbolin-1-one

Chemical Property:

• Vapor Pressure: 4.11E-12mmHg at 25°C
• Boiling Point: 549.2°C at 760 mmHg
• Flash Point: 286°C
• Density: 1.308g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-methoxy-2,3,4,9-tetrahydro-1H-beta-carbolin-1-one

There total 1 articles about 7-methoxy-2,3,4,9-tetrahydro-1H-beta-carbolin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

harmaline (304-21-2) → harmine (442-51-3) + 7-methoxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-one (26579-69-1) + oxoharmaline A + oxoharmaline B + oxoharmaline C + oxoharmaline D + N-[3-[2-(formylamino)-4-methoxyphenyl]-3-oxopropyl]acetamide

Guidance literature:

With riboflavin; In methanol; acetonitrile; UV-irradiation;

DOI:10.1016/j.fitote.2021.105054

Reference yield: 100.0%

7-methoxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-one (26579-69-1) → 7-methoxy-1,2,3,4-tetrahydro-β-carboline (91566-22-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran;

Reference yield: 90.0%

7-methoxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-one (26579-69-1) → 6-methoxytryptamine-2-carboxylic acid (20731-72-0)

Guidance literature:

With potassium hydroxide; Heating; 2-3 h;

DOI:10.1021/jo00001a066

upstream raw materials:

harmaline

Downstream raw materials:

6-methoxytryptamine-2-carboxylic acid

7-methoxy-1,2,3,4-tetrahydro-β-carboline

CGS 19281A

2-(6-methoxy-1H-indol-3-yl)ethanamine

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