2-phenyl-6-heptenohydroximoyl bromide

Base Information

Chemical Name:2-phenyl-6-heptenohydroximoyl bromide
CAS No.:202061-77-6
Molecular Formula:C₁₃H₁₆BrNO
Molecular Weight:282.18
Hs Code.:

Synonyms:2-phenyl-6-heptenohydroximoyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenyl-6-heptenohydroximoyl bromide

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Technology Process of 2-phenyl-6-heptenohydroximoyl bromide

There total 3 articles about 2-phenyl-6-heptenohydroximoyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₁₃H₁₆NO₂^(1-)*Br^(1-)*Mg⁽²⁺⁾

: (3aS,7R)-7-Phenyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole

: (3aR,7R)-7-Phenyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole

: 202061-77-6
2-phenyl-6-heptenohydroximoyl bromide

Guidance literature:: With hydrogen bromide; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1016/S0040-4020(99)00351-8

Reference yield:

: 5153-67-3
nitrostyrene

: 34164-50-6
4-penten-1-ylmagnesium bromide

: 202061-77-6
2-phenyl-6-heptenohydroximoyl bromide

Guidance literature:: nitrostyrene; 4-penten-1-ylmagnesium bromide; at -20 ℃; for 0.5h;

With hydrogen bromide; for 0.5h; ice cooling;
DOI:10.1016/S0040-4020(97)10356-8