ethyl 3-([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)-3-oxopropanoate

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Chemical Name:ethyl 3-([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)-3-oxopropanoate
CAS No.:938447-20-2
Molecular Formula:C₂₈H₃₃N₃O₇S
Molecular Weight:555.652
Hs Code.:

Synonyms:ethyl 3-([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)-3-oxopropanoate

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Chemical Property of ethyl 3-([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)-3-oxopropanoate

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Technology Process of ethyl 3-([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)-3-oxopropanoate

There total 1 articles about ethyl 3-([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 938447-12-2
3-[(E)-3-({1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)prop-1-enyl]benzonitrile

: 36239-09-5
ethyl chlorocarbonylacetate

: 938447-20-2
ethyl 3-([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)-3-oxopropanoate

Guidance literature:: With triethylamine; In 1,2-dichloro-ethane; at 0 ℃; for 3h;
DOI:10.1016/j.bmc.2007.03.066

Reference yield: 74.0%

: 938447-20-2
ethyl 3-([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)-3-oxopropanoate

: ethyl (((E)-3-{3-[amino(imino)methyl]phenyl}prop-2-enyl){1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)-3-oxopropanoate hydrochloride

Guidance literature:: ethyl 3-([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)-3-oxopropanoate; With hydrogenchloride; In ethanol; chloroform; at 5 ℃; for 22h;

With ammonium acetate; In ethanol; at 20 ℃; for 24h; Further stages.;
DOI:10.1016/j.bmc.2007.03.066