p-methoxybenzyl 4-O-acetyl-2,3,6-trideoxy-α-L-arabino-hex-2-enopyranoside

Base Information

Chemical Name:p-methoxybenzyl 4-O-acetyl-2,3,6-trideoxy-α-L-arabino-hex-2-enopyranoside
CAS No.:452071-57-7
Molecular Formula:C₁₆H₂₀O₅
Molecular Weight:292.332
Hs Code.:

Synonyms:p-methoxybenzyl 4-O-acetyl-2,3,6-trideoxy-α-L-arabino-hex-2-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxybenzyl 4-O-acetyl-2,3,6-trideoxy-α-L-arabino-hex-2-enopyranoside

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Technology Process of p-methoxybenzyl 4-O-acetyl-2,3,6-trideoxy-α-L-arabino-hex-2-enopyranoside

There total 1 articles about p-methoxybenzyl 4-O-acetyl-2,3,6-trideoxy-α-L-arabino-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 105-13-5
4-Methoxybenzyl alcohol

: 34819-86-8
3,4-di-O-acetyl-6-deoxy-L-glucal

: 452071-57-7
p-methoxybenzyl 4-O-acetyl-2,3,6-trideoxy-α-L-arabino-hex-2-enopyranoside

Guidance literature:: With tin(IV) chloride; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1016/S0968-0896(01)00411-4

Reference yield: 90.0%

: 452071-57-7
p-methoxybenzyl 4-O-acetyl-2,3,6-trideoxy-α-L-arabino-hex-2-enopyranoside

: 452071-58-8
p-methoxybenzyl 4-O-acetyl-2,3,6-trideoxy-α-L-arabino-hexopyranoside

Guidance literature:: With hydrogen; Wilkinson's catalyst; In benzene; for 2h; under 760 Torr;
DOI:10.1016/S0968-0896(01)00411-4

Reference yield:

: 452071-57-7
p-methoxybenzyl 4-O-acetyl-2,3,6-trideoxy-α-L-arabino-hex-2-enopyranoside

: 452071-59-9
p-methoxybenzyl 2,3,6-trideoxy-α-L-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / H₂ / (Ph₃P)3RhCl / benzene / 2 h / 760 Torr

2: 60 percent / NaOMe / methanol / 2 h / 20 °C

With hydrogen; sodium methylate; Wilkinson's catalyst; In methanol; benzene;
DOI:10.1016/S0968-0896(01)00411-4