2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine

Base Information

Chemical Name:2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine
CAS No.:1245819-13-9
Molecular Formula:C₂₅H₃₃N₅O₁₀Si
Molecular Weight:591.65
Hs Code.:

2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N<sup>4</sup>-acetylarabinocytidine

Synonyms:2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine

Suppliers and Price of 2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine

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Technology Process of 2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine

There total 3 articles about 2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1245819-05-9
3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 1245819-13-9
2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at -30 ℃; for 3h;
DOI:10.1080/15257770.2010.507233

Reference yield:

: 13491-47-9
N₄-acetyl-4-amino-1-[(2R,3S,4S,5R)-3,4-dihydroxy-5-(hydroxymethyl)oxolan-2-yl]pyrimidin-2-one

: 1245819-13-9
2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 0 - 20 °C

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / -30 °C

With 2,6-dimethylpyridine; sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1080/15257770.2010.507233

Reference yield:

: 147-94-4
arabinosyl cytosine

: 1245819-13-9
2'-O-(2,4-dinitrophenyl)-3',5'-O-di-tert-butylsilyl-N⁴-acetylarabinocytidine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 3 h / Reflux

2: 2,6-dimethylpyridine / N,N-dimethyl-formamide / 0 - 20 °C

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / -30 °C

With 2,6-dimethylpyridine; sodium hydride; In methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1080/15257770.2010.507233