(1R,3R,4R)-4-Benzyloxymethoxy-3-methoxy-cyclohexanecarboxylic acid isopropyl ester

Base Information

Chemical Name:(1R,3R,4R)-4-Benzyloxymethoxy-3-methoxy-cyclohexanecarboxylic acid isopropyl ester
CAS No.:201993-91-1
Molecular Formula:C₁₉H₂₈O₅
Molecular Weight:336.428
Hs Code.:

Synonyms:(1R,3R,4R)-4-Benzyloxymethoxy-3-methoxy-cyclohexanecarboxylic acid isopropyl ester

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Chemical Property of (1R,3R,4R)-4-Benzyloxymethoxy-3-methoxy-cyclohexanecarboxylic acid isopropyl ester

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Technology Process of (1R,3R,4R)-4-Benzyloxymethoxy-3-methoxy-cyclohexanecarboxylic acid isopropyl ester

There total 5 articles about (1R,3R,4R)-4-Benzyloxymethoxy-3-methoxy-cyclohexanecarboxylic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 201993-91-1
(1R,3R,4R)-4-Benzyloxymethoxy-3-methoxy-cyclohexanecarboxylic acid isopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N

2: 93 percent / iPrONa

3: NaH / tetrahydrofuran

With sodium isopropylate; sodium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1016/S0040-4039(97)10532-9

Reference yield:

: 116498-92-1
(1R,4R,5R)-4-hydroxy-6-oxabicyclo[3.2.1]octan-7-one

: 201993-91-1
(1R,3R,4R)-4-Benzyloxymethoxy-3-methoxy-cyclohexanecarboxylic acid isopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N

2: 93 percent / iPrONa

3: NaH / tetrahydrofuran

With sodium isopropylate; sodium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1016/S0040-4039(97)10532-9

Reference yield:

: 201993-84-2
Trifluoro-acetic acid (1R,4R,5R)-7-oxo-6-oxa-bicyclo[3.2.1]oct-4-yl ester

: 201993-91-1
(1R,3R,4R)-4-Benzyloxymethoxy-3-methoxy-cyclohexanecarboxylic acid isopropyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: silicagel, Na₂CO₃ / tetrahydrofuran; various solvent(s) / pH 8

2: Et₃N

3: 93 percent / iPrONa

4: NaH / tetrahydrofuran

With sodium isopropylate; silica gel; sodium hydride; sodium carbonate; triethylamine; In tetrahydrofuran;
DOI:10.1016/S0040-4039(97)10532-9