2-(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1383710-31-3
Molecular Formula:C₂₂H₃₇BO₄
Molecular Weight:376.344
Hs Code.:

Synonyms:2-(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about 2-(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1-bromo-3,5-di-tert-butyl-2-(methoxymethoxy)benzene

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1383710-31-3
2-(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: 1-bromo-3,5-di-tert-butyl-2-(methoxymethoxy)benzene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.5h; Inert atmosphere; Cooling with acetone-dry ice;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In diethyl ether; hexane; at -78 - 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1039/c2cc32806b

Reference yield: 82.0%

: 626-05-1
2,6-Dibromopyridine

: 1383710-31-3
2-(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1015257-41-6
2,6-bis(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)pyridine

: 1383710-28-8
2-bromo-6-(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)pyridine

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 20 - 115 ℃; for 168h; Inert atmosphere;
DOI:10.1039/c2cc32806b

Reference yield: 45.0%

: 626-05-1
2,6-Dibromopyridine

: 1383710-31-3
2-(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1015257-41-6
2,6-bis(3,5-di-tert-butyl-2-(methoxymethoxy)phenyl)pyridine

Guidance literature:: With {1,3-bis[2,6-bis(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}dichloro(pyridine)palladium; potassium tert-butylate; In isopropyl alcohol; at 24 ℃; for 48h; Schlenk technique;
DOI:10.1021/jacs.9b01805