ethyl 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzimidate hydrochloride

Base Information

Chemical Name:ethyl 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzimidate hydrochloride
CAS No.:1346427-99-3
Molecular Formula:C₁₄H₂₁NO₅*ClH
Molecular Weight:319.785
Hs Code.:

Synonyms:ethyl 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzimidate hydrochloride

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Chemical Property of ethyl 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzimidate hydrochloride

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Technology Process of ethyl 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzimidate hydrochloride

There total 3 articles about ethyl 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzimidate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-17-5
ethanol

: 1346427-97-1
2-hydroxy-3-(3,6-dioxaheptyloxy)benzonitrile

: 1346427-99-3
ethyl 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzimidate hydrochloride

Guidance literature:: With hydrogenchloride; at 40 ℃;

Reference yield:

: 50586-80-6,58320-73-3
toluene-4-sulfonic acid 2-(2-methoxyethoxy)ethyl ester

: 1346427-99-3
ethyl 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzimidate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 1 h / 60 °C

1.2: 1 h / 60 °C

2.1: hydrogenchloride / 40 °C

With hydrogenchloride; sodium hydride; In dimethyl sulfoxide; mineral oil;

Reference yield:

: 67984-81-0
2,3-dihydroxybenzonitrile

: 1346427-99-3
ethyl 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzimidate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 1 h / 60 °C

1.2: 1 h / 60 °C

2.1: hydrogenchloride / 40 °C

With hydrogenchloride; sodium hydride; In dimethyl sulfoxide; mineral oil;