C₃₃H₃₉NO₅

Base Information

Chemical Name:C₃₃H₃₉NO₅
CAS No.:1234693-22-1
Molecular Formula:C₃₃H₃₉NO₅
Molecular Weight:529.676
Hs Code.:

C<sub>33</sub>H<sub>39</sub>NO<sub>5</sub>

Synonyms:C₃₃H₃₉NO₅

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Chemical Property of C₃₃H₃₉NO₅

Chemical Property:

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Technology Process of C₃₃H₃₉NO₅

There total 2 articles about C₃₃H₃₉NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 201230-82-2
carbon monoxide

: 1099752-19-8
tert-butyl formyl{(1S)-1-[(trityloxy)methyl]prop-2-enyl}carbamate

: 1439-36-7
1-triphenylphosphoranylidene-2-propanone

: 1234693-22-1
C₃₃H₃₉NO₅

: 1234693-12-9
C₃₃H₃₇NO₅

Guidance literature:: With (acetylacetonato)dicarbonylrhodium (l); hydrogen; 6,6′-[(3,3′-di-tert-butyl-5,5′-dimethoxy-1,1′-biphenyl-2,2′-diyl)bis(oxy)]bis(di-benzo[d,f][1,3,2]dioxaphosphepin); In toluene; at 50 ℃; for 13h; under 750.075 Torr; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201000016

Reference yield:

: 201230-82-2
carbon monoxide

: 1099752-19-8
tert-butyl formyl{(1S)-1-[(trityloxy)methyl]prop-2-enyl}carbamate

: 1439-36-7
1-triphenylphosphoranylidene-2-propanone

: 1234693-22-1
C₃₃H₃₉NO₅

Guidance literature:: carbon monoxide; tert-butyl formyl{(1S)-1-[(trityloxy)methyl]prop-2-enyl}carbamate; 1-triphenylphosphoranylidene-2-propanone; With (acetylacetonato)dicarbonylrhodium (l); hydrogen; 6,6′-[(3,3′-di-tert-butyl-5,5′-dimethoxy-1,1′-biphenyl-2,2′-diyl)bis(oxy)]bis(di-benzo[d,f][1,3,2]dioxaphosphepin); In toluene; at 50 ℃; for 13h; under 750.075 Torr; Inert atmosphere;

With Pd(OH)2/C; hydrogen; In ethyl acetate; at 20 ℃; for 1h; under 760.051 Torr; Inert atmosphere;
DOI:10.1002/adsc.201000016