Technology Process of C31H37ClN2O5
There total 4 articles about C31H37ClN2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-chloro-3,4-bis[(4-methoxyphenyl)methoxy]benzoic acid;
With
methanesulfonyl chloride; triethylamine;
In
N,N-dimethyl acetamide;
at -15 ℃;
for 1h;
2-(azepan-1-yl)ethanamine hydrochloride;
In
N,N-dimethyl acetamide;
for 1h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 3 h / 70 °C
2.1: sodium hydroxide; water / tetrahydrofuran; methanol / 1.33 h / 70 °C
3.1: triethylamine; methanesulfonyl chloride / N,N-dimethyl acetamide / 1 h / -15 °C
3.2: 1 h
With
water; potassium carbonate; methanesulfonyl chloride; triethylamine; sodium iodide; sodium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydroxide; water / tetrahydrofuran; methanol / 1.33 h / 70 °C
2.1: triethylamine; methanesulfonyl chloride / N,N-dimethyl acetamide / 1 h / -15 °C
2.2: 1 h
With
water; methanesulfonyl chloride; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl acetamide;