(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-(benzyl-t-butyloxycarbonylamino)hex-2-enyl ester

Base Information

Chemical Name:(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-(benzyl-t-butyloxycarbonylamino)hex-2-enyl ester
CAS No.:960060-50-8
Molecular Formula:C₂₈H₃₅F₃N₂O₄
Molecular Weight:520.592
Hs Code.:

Synonyms:(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-(benzyl-t-butyloxycarbonylamino)hex-2-enyl ester

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Chemical Property of (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-(benzyl-t-butyloxycarbonylamino)hex-2-enyl ester

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Technology Process of (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-(benzyl-t-butyloxycarbonylamino)hex-2-enyl ester

There total 1 articles about (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-(benzyl-t-butyloxycarbonylamino)hex-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 960060-32-6
tert-butyl (E)-benzyl(6-hydroxy-4-methylhex-4-en-1-yl)carbamate

: 75999-66-5
N-(4-methoxyphenyl)trifluoroacetimidoyl chloride

: 960060-50-8
(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-(benzyl-t-butyloxycarbonylamino)hex-2-enyl ester

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -50 - -20 ℃; Inert atmosphere;
DOI:10.1002/chem.200900712

Reference yield: 64.0%

: 960060-50-8
(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-(benzyl-t-butyloxycarbonylamino)hex-2-enyl ester

: 960060-64-4
(R)-tert-butyl benzyl-(4-methyl-4-(2,2,2-trifluoro-N-(4-methoxyphenyl)acetamido)hex-5-enyl)carbamate

Guidance literature:: With di-μ-chlorobis[η⁵-(4'R,5'R)-(S_p)-2-(2'-4',5'-dihydro-4',5'-diphenyl-1'-tosyl-1'H-imidazolyl)cyclopentadienyl, (1-C,3'-N)(η⁵-pentaphenylcyclopentadienyl)-iron(II)]dipalladium(II); silver trifluoroacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In dichloromethane; at 50 ℃; for 60h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900712