(R)-tert-butyl benzyl-(4-methyl-4-(2,2,2-trifluoro-N-(4-methoxyphenyl)acetamido)hex-5-enyl)carbamate

Base Information

Chemical Name:(R)-tert-butyl benzyl-(4-methyl-4-(2,2,2-trifluoro-N-(4-methoxyphenyl)acetamido)hex-5-enyl)carbamate
CAS No.:960060-64-4
Molecular Formula:C₂₈H₃₅F₃N₂O₄
Molecular Weight:520.592
Hs Code.:

Synonyms:(R)-tert-butyl benzyl-(4-methyl-4-(2,2,2-trifluoro-N-(4-methoxyphenyl)acetamido)hex-5-enyl)carbamate

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Chemical Property of (R)-tert-butyl benzyl-(4-methyl-4-(2,2,2-trifluoro-N-(4-methoxyphenyl)acetamido)hex-5-enyl)carbamate

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Technology Process of (R)-tert-butyl benzyl-(4-methyl-4-(2,2,2-trifluoro-N-(4-methoxyphenyl)acetamido)hex-5-enyl)carbamate

There total 2 articles about (R)-tert-butyl benzyl-(4-methyl-4-(2,2,2-trifluoro-N-(4-methoxyphenyl)acetamido)hex-5-enyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 960060-50-8
(E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-(benzyl-t-butyloxycarbonylamino)hex-2-enyl ester

: 960060-64-4
(R)-tert-butyl benzyl-(4-methyl-4-(2,2,2-trifluoro-N-(4-methoxyphenyl)acetamido)hex-5-enyl)carbamate

Guidance literature:: With di-μ-chlorobis[η⁵-(4'R,5'R)-(S_p)-2-(2'-4',5'-dihydro-4',5'-diphenyl-1'-tosyl-1'H-imidazolyl)cyclopentadienyl, (1-C,3'-N)(η⁵-pentaphenylcyclopentadienyl)-iron(II)]dipalladium(II); silver trifluoroacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In dichloromethane; at 50 ℃; for 60h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900712

Reference yield:

: (E)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidic acid 3-methyl-6-(benzyl-t-butyloxycarbonylamino)hex-2-enyl ester

: C₂₈H₃₅F₃N₂O₄

: 960060-64-4
(R)-tert-butyl benzyl-(4-methyl-4-(2,2,2-trifluoro-N-(4-methoxyphenyl)acetamido)hex-5-enyl)carbamate

Guidance literature:: With silver trifluoroacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; ferrocenyl 1-Ts-2,3-Ph₂-imidazoline palladacycle catalyst; In dichloromethane; at 50 ℃; for 60h; Title compound not separated from byproducts.;
DOI:10.1002/anie.200702086