3',5'-di-O-acetyl-2'-deoxy-O²,O⁶-bis-[2-(4-nitrophenyl)ethyl]xanthosine

Base Information

Chemical Name:3',5'-di-O-acetyl-2'-deoxy-O²,O⁶-bis-[2-(4-nitrophenyl)ethyl]xanthosine
CAS No.:292050-44-3
Molecular Formula:C₃₀H₃₀N₆O₁₁
Molecular Weight:650.602
Hs Code.:

3',5'-di-O-acetyl-2'-deoxy-O<sup>2</sup>,O<sup>6</sup>-bis-[2-(4-nitrophenyl)ethyl]xanthosine

Synonyms:3',5'-di-O-acetyl-2'-deoxy-O²,O⁶-bis-[2-(4-nitrophenyl)ethyl]xanthosine

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Chemical Property of 3',5'-di-O-acetyl-2'-deoxy-O²,O⁶-bis-[2-(4-nitrophenyl)ethyl]xanthosine

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Technology Process of 3',5'-di-O-acetyl-2'-deoxy-O²,O⁶-bis-[2-(4-nitrophenyl)ethyl]xanthosine

There total 3 articles about 3',5'-di-O-acetyl-2'-deoxy-O²,O⁶-bis-[2-(4-nitrophenyl)ethyl]xanthosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 20264-96-4
2-(4-nitrophenyl)ethyl iodide

: 108310-93-6
3',5'-di-O-acetyl-2'-deoxy-O⁶-[2-(4-nitrophenyl)ethyl]xanthosine

: 292050-44-3
3',5'-di-O-acetyl-2'-deoxy-O²,O⁶-bis-[2-(4-nitrophenyl)ethyl]xanthosine

Guidance literature:: 3',5'-di-O-acetyl-2'-deoxy-O⁶-[2-(4-nitrophenyl)ethyl]xanthosine; With silver carbonate; In benzene; for 1h; Heating;

2-(4-nitrophenyl)ethyl iodide; In benzene; at 50 ℃; for 15h;
DOI:10.1002/1522-2675(20000705)83:7<1517::AID-HLCA1517>3.0.CO;2-S

Reference yield:

: 108310-92-5
2-amino-6-(2-(p-nitrophenyl)ethyloxy)-9-[2'-deoxy-β-D-erythropentofuranosyl]purine diacetate

: 292050-44-3
3',5'-di-O-acetyl-2'-deoxy-O²,O⁶-bis-[2-(4-nitrophenyl)ethyl]xanthosine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 57 percent / NaNO₂; AcOH

2.1: Ag₂CO₃ / benzene / 1 h / Heating

2.2: 93 percent / benzene / 15 h / 50 °C

With acetic acid; silver carbonate; sodium nitrite; In benzene; 1.1: Oxidation / 2.1: Reduction / 2.2: Substitution;
DOI:10.1002/1522-2675(20000705)83:7<1517::AID-HLCA1517>3.0.CO;2-S