methyl 2-{methyl[3-(4-nitrophenyl)prop-2-yn-1-yl]amino}-2-(trifluoromethyl)pent-4-enoate

Base Information

Chemical Name:methyl 2-{methyl[3-(4-nitrophenyl)prop-2-yn-1-yl]amino}-2-(trifluoromethyl)pent-4-enoate
CAS No.:1456821-85-4
Molecular Formula:C₁₇H₁₇F₃N₂O₄
Molecular Weight:370.328
Hs Code.:

Synonyms:methyl 2-{methyl[3-(4-nitrophenyl)prop-2-yn-1-yl]amino}-2-(trifluoromethyl)pent-4-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-{methyl[3-(4-nitrophenyl)prop-2-yn-1-yl]amino}-2-(trifluoromethyl)pent-4-enoate

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Technology Process of methyl 2-{methyl[3-(4-nitrophenyl)prop-2-yn-1-yl]amino}-2-(trifluoromethyl)pent-4-enoate

There total 1 articles about methyl 2-{methyl[3-(4-nitrophenyl)prop-2-yn-1-yl]amino}-2-(trifluoromethyl)pent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 636-98-6
p-nitrobenzene iodide

: C₁₂H₁₆F₃NO₂

: 1456821-85-4
methyl 2-{methyl[3-(4-nitrophenyl)prop-2-yn-1-yl]amino}-2-(trifluoromethyl)pent-4-enoate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at -50 - 20 ℃; for 4h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.201300619

Reference yield: 60.0%

: 1456821-85-4
methyl 2-{methyl[3-(4-nitrophenyl)prop-2-yn-1-yl]amino}-2-(trifluoromethyl)pent-4-enoate

: 1456821-95-6
methyl 1-methyl-5-[1-(4-nitrophenyl)vinyl]-2-(trifluoromethyl)-1,2,3,6-tetrahydropyridine-2-carboxylate

: 1456821-96-7
methyl 1-methyl-6-methylene-5-(4-nitrophenyl)-2-(trifluoromethyl)-2,3,6,7-tetrahydro-1H-azepine-2-carboxylate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 80 ℃; for 2h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.201300619