C₅₀H₆₅N₁₃O₁₁

Base Information

Chemical Name:C₅₀H₆₅N₁₃O₁₁
CAS No.:1203557-02-1
Molecular Formula:C₅₀H₆₅N₁₃O₁₁
Molecular Weight:1024.15
Hs Code.:

C<sub>50</sub>H<sub>65</sub>N<sub>13</sub>O<sub>11</sub>

Synonyms:C₅₀H₆₅N₁₃O₁₁

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Chemical Property of C₅₀H₆₅N₁₃O₁₁

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Technology Process of C₅₀H₆₅N₁₃O₁₁

There total 13 articles about C₅₀H₆₅N₁₃O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₀H₆₇N₁₃O₁₂

: 1203557-02-1
C₅₀H₆₅N₁₃O₁₁

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1016/j.ejmech.2012.01.054

Reference yield:

: 84520-68-3
N-tert-butoxycarbonyl-cis-4-azido-L-proline methyl ester

: 1203557-02-1
C₅₀H₆₅N₁₃O₁₁

Guidance literature:: Multi-step reaction with 11 steps

1.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C

2.2: 25 h / 0 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 0 - 20 °C

5.1: diethylamine / dichloromethane / 2 h / Cooling with ice

6.1: dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C

6.2: 48 h / 20 °C

7.1: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

8.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C

9.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

10.1: sodium hydroxide / ethanol / 20 °C

10.2: pH 7

11.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C

With dmap; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.01.054

Reference yield:

: 772327-98-7
(2S,4S)-1-((2S,3R)-2-Amino-3-hydroxy-butyryl)-4-azido-pyrrolidine-2-carboxylic acid methyl ester

: 1203557-02-1
C₅₀H₆₅N₁₃O₁₁

Guidance literature:: Multi-step reaction with 6 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 24.67 h / 0 - 20 °C

2.1: sodium hydroxide / ethanol / 24 h / 20 °C

2.2: pH 4.5

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

5.1: sodium hydroxide / ethanol / 20 °C

5.2: pH 7

6.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.01.054