Benzoic acid (S)-2-bromo-1-((2S,3S,4S)-4-bromo-3-hydroxy-5-oxo-tetrahydro-furan-2-yl)-ethyl ester

Base Information

Chemical Name:Benzoic acid (S)-2-bromo-1-((2S,3S,4S)-4-bromo-3-hydroxy-5-oxo-tetrahydro-furan-2-yl)-ethyl ester
CAS No.:98120-39-9
Molecular Formula:C₁₃H₁₂Br₂O₅
Molecular Weight:408.043
Hs Code.:

Synonyms:Benzoic acid (S)-2-bromo-1-((2S,3S,4S)-4-bromo-3-hydroxy-5-oxo-tetrahydro-furan-2-yl)-ethyl ester

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Chemical Property of Benzoic acid (S)-2-bromo-1-((2S,3S,4S)-4-bromo-3-hydroxy-5-oxo-tetrahydro-furan-2-yl)-ethyl ester

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Technology Process of Benzoic acid (S)-2-bromo-1-((2S,3S,4S)-4-bromo-3-hydroxy-5-oxo-tetrahydro-furan-2-yl)-ethyl ester

There total 1 articles about Benzoic acid (S)-2-bromo-1-((2S,3S,4S)-4-bromo-3-hydroxy-5-oxo-tetrahydro-furan-2-yl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 69617-72-7
(3S,4S,5R,1'S)-3-bromo-5-(2'-bromo-1'-hydroxy)ethyl-4,5-dihydro-4-hydroxy-2-(3H)-furanone

: 98-88-4
benzoyl chloride

: 98120-39-9
Benzoic acid (S)-2-bromo-1-((2S,3S,4S)-4-bromo-3-hydroxy-5-oxo-tetrahydro-furan-2-yl)-ethyl ester

Guidance literature:: In pyridine; at -30 - -10 ℃; for 1h;
DOI:10.1016/0008-6215(85)85201-0

Reference yield: 90.0%

: 109-87-5
Dimethoxymethane

: 98120-39-9
Benzoic acid (S)-2-bromo-1-((2S,3S,4S)-4-bromo-3-hydroxy-5-oxo-tetrahydro-furan-2-yl)-ethyl ester

: 98120-40-2
5-O-benzoyl-2,6-dibromo-2,6-dideoxy-3-O-methoxymethyl-D-mannono-1,4-lactone

Guidance literature:: With phosphorus pentoxide; In dichloromethane; for 0.25h;
DOI:10.1016/0008-6215(85)85201-0

Reference yield:

: 98120-39-9
Benzoic acid (S)-2-bromo-1-((2S,3S,4S)-4-bromo-3-hydroxy-5-oxo-tetrahydro-furan-2-yl)-ethyl ester

: (3R,4R)-5-(1,3-Diphenyl-imidazolidin-2-yl)-4-methoxymethoxy-pent-1-en-3-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / P₂O₅ / CH₂Cl₂ / 0.25 h

2: 87 percent / zinc-silver couple / ethanol; H₂O / 8 h / 20 °C

3: 81 percent / di-isobutylaluminiumhydride / CH₂Cl₂ / 0.33 h / -78 °C

4: methanol / 5 h / Heating

With diisobutylaluminum hydride; zinc silver; phosphorus pentoxide; In methanol; ethanol; dichloromethane; water;
DOI:10.1016/0008-6215(85)85201-0