Technology Process of C31H33Cl3N2O6
There total 9 articles about C31H33Cl3N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
dichloromethane;
at 20 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: tetra-(n-butyl)ammonium iodide / dimethyl sulfoxide / 110 °C
2: acetyl chloride / 5 - 20 °C
3: hydrazine / ethanol / 80 °C
4: pyridine / 20 °C
5: methanol; sodium methylate / 20 °C
6: sodium hydride / N,N-dimethyl-formamide / 10 - 25 °C
7: hydrogenchloride; water / acetic acid / 75 °C
8: potassium carbonate / dichloromethane / 12 h / 20 °C
With
pyridine; hydrogenchloride; methanol; water; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; acetyl chloride; hydrazine;
In
ethanol; dichloromethane; acetic acid; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / 20 °C
2: methanol; sodium methylate / 20 °C
3: sodium hydride / N,N-dimethyl-formamide / 10 - 25 °C
4: hydrogenchloride; water / acetic acid / 75 °C
5: potassium carbonate / dichloromethane / 12 h / 20 °C
With
pyridine; hydrogenchloride; methanol; water; sodium methylate; sodium hydride; potassium carbonate;
In
dichloromethane; acetic acid; N,N-dimethyl-formamide;